室内空气中二氧化碳的测定方法（Method of determination of carbon dioxide in indoor air）.doc

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室内空气中二氧化碳的测定方法（Method of determination of carbon dioxide in indoor air）.doc

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室内空气中二氧化碳的测定方法（Method of determination of carbon dioxide in indoor air） Method of determination of carbon dioxide in indoor air The methods of determination of carbon dioxide in air mainly include non-disperse infrared gas analysis, gas chromatography, volumetric titration and so on. E. 1 nondispersive infrared gas analysis E. 1.1 relevant standards and basis The method is mainly based on GB/T18204.24 method of determination of carbon dioxide in public places. E. 1.2 principle Carbon dioxide has a selective absorption of infrared ray. In a certain range, the absorption value is linear with the concentration of carbon dioxide. The concentration of the sample carbon dioxide is determined according to the absorption value. E. 1.3 measurement range 0 ~ 0.5%; Between 0 and 1.5 %. The minimum detectable concentration was 0.01%. E. 1.4 reagents and materials E. 1.4.1 color silica gel: dry 2 h under 120 ℃; E. 1.4.2 non-aqueous calcium chloride: analytical pure; E. 1.4.3 high purity nitrogen: 99.99% purity; E. 1.4.4 caustic asbestos: analytical pure; E. 1.4.5 plastic aluminum foil composite film mining bag 0.5l or 1.0l; E. 1.4.6 co2 standard gas (0.5%) : stored in aluminum alloy cylinders. E. 1.5 instruments and equipment Carbon dioxide nondispersive infrared gas analyzer. The main performance indexes of the instrument are as follows: Measurement range: 0 ~ 0.5%; Two 0 ~ 1.5%; Reproducibility: less than or less than 1% full scale; Zero drift: no more than or minus 3% full scale / 4h; Span drift: no more than or minus 3% full scale / 4h; Additional temperature error: + / - 2% of full scale / 10 ℃ or less (10 ℃ ~ 80 ℃); Carbon monoxide interference: 1000mL/m3 CO. Additional error: 220V plus or minus 10% is equal to or minus 2% full scale. Starting time: 30min; Response time: the pointer indicates the full scale of 90% of the time 15s. E. 1.6 sampling Using plastic aluminum foil compound film to collect air bags, extract the air flush 3 ~ 4 times, gas extraction 0.5 L or 1.0 L