自蔓延高温合成内衬陶瓷复合涂层的制备及研究.PDFVIP

下半月出版 Material Heat Treatment 料热处理技术 自蔓延高温合成内衬陶瓷复合涂层的制备及研究 王欣1 2 1 1 , 陈志兵 , 刘鹏 , 孙广合 (1.中国铁道科学研究院机车车辆研究所袁北京100081 曰2. 北京市轨道交通建设管理有限公司袁北京100037) 摘 要 采用自蔓延高温合成技术在钢管内制备陶瓷涂层 并对涂层的组织和性能进行了分析遥 结果表明院涂层从 内到外依次为刚玉陶瓷层和以铁为主的过渡层 涂层的显微组织呈枝晶状结构 白色相为Al O 黑色部分主要为Fe 和 2 3 Fe 尧Al 合成相曰涂层的断口为层片状结构 层片界面有气孔或裂纹曰断口较平坦 呈解理台阶 为脆性断裂遥 涂层结合强 高 耐冲蚀性能优良遥 关键词 陶瓷内衬涂层曰显微组织曰性能 中图分类号 TB331 文献标识码 A 文章编号 Research on Ceramic-lined Coating Prepared by Self-propagating High-temperature Synthesis 1 2 1 1 WANG Xin , CHEN Zhibing , LIU Peng , SUN Guanghe (1. Locomotiv e Rolling Institute, China Railway Scientific Research Institute, Be ij ing 100081, China; 2. Beij ing Urban Rail Traffic Cons truc tion Manageme nt Co., Ltd., Be ij ing 100037, China) Abstract 院The ceramic coating was prepared in the steel tube by the self-propagating high-temperature synthesis technique. The microstructure and properties of coating were analyzed. The results show that the coating is orderly corundum ceramic layer and intermediate layer with iron mainly from inside to outside. The microscopic structures of the coating are branch crystalline structure; the white phase is Al2O3 and the black phase is Fe and the synthesis phase of Fe and Al. The fracture of the coati