结晶与重结晶（Crystallization and recrystallization）.docVIP

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结晶与重结晶（Crystallization and recrystallization）.doc

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结晶与重结晶（Crystallization and recrystallization）

结晶与重结晶（Crystallization and recrystallization） Crystallization and recrystallization The difference of crystal shape of compound directly influences its stability / speed of absorption / moisture absorption / purity, etc. General principles for selection of crystalline solvents and methods for determining crystalline purity. The general principle of choice of crystallization solvent: the solubility of the components to be heated is large, the solubility is small when cold, and the impurities are neither hot nor cold, or hot and cold are soluble. Boiling point should be appropriate, should not be too high or too low, such as ether should not be used. Or the use of substances and impurities in different solvents in the solvent difference, select solvents The method of determining crystal purity: homogeneous physical and chemical properties; solid compound melting distance Less than or equal to 2 DEG C; TLC or PC launched a single spot; HPLC or GC analysis showed a single peak Modern crystallography mainly includes the following several branches: (1) crystal forming Science (crystallogeny): study the process and mechanism of the occurrence, growth and change of natural and artificial crystals, and the factors that control and influence them. (2) (gometrical Crystallography): Geometric crystallography regularity during the study of crystal shape and appearance of geometric polyhedron. (3) crystal structure (crystallology): study the regularity of particle arrangement in crystal internal structure, and the imperfection of crystal structure. (4) crystal chemistry (crystallochemistry, also known as crystal chemistry): the study of the relation between chemical composition and crystal structure, as well as the physical and chemical properties of crystals. (5) crystal physics (crystallophysics): study the physical properties of crystals and their mechanisms. Thj Id like to discuss some of my views: Solvent: the key to the preparation of crystallization. In addition to the men