facile synthesis of highly aligned multiwalled carbon nanotubes from polymer precursors简单合成高度一致的微碳纳米管聚合物前体.pdfVIP

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facile synthesis of highly aligned multiwalled carbon nanotubes from polymer precursors简单合成高度一致的微碳纳米管聚合物前体.pdf

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facile synthesis of highly aligned multiwalled carbon nanotubes from polymer precursors简单合成高度一致的微碳纳米管聚合物前体

Hindawi Publishing Corporation Journal of Nanomaterials Volume 2009, Article ID 562376, 11 pages doi:10.1155/2009/562376 Research Article Facile Synthesis of Highly Aligned Multiwalled Carbon Nanotubes from Polymer Precursors Catherine Y. Han,1, 2 Zhi-Li Xiao,1, 3 H. Hau Wang,1 Xiao-Min Lin,4 Susana Trasobares,1, 5 and Russell E. Cook1 1 Materials Science Division, Argonne National Laboratory, Argonne, IL 60439, USA 2 Physical Science Department, Richard J. Daley College, Chicago, IL 60652, USA 3 Department of Physics, Northern Illinois University, DeKalb, IL 60115, USA 4 Center for Nanoscale Materials, Argonne National Laboratory, Argonne, IL 60439, USA 5 Departamento de Ciencia de Materiales, Universidad de Cadiz, Puerto Real 11510 Cadiz, Spain Correspondence should be addressed to H. Hau Wang, hau.wang@ Received 11 November 2008; Accepted 25 February 2009 Recommended by Jun Liu We report a facile one-step approach which involves no ﬂammable gas, no catalyst, and no in situ polymerization for the preparation of well-aligned carbon nanotube array. A polymer precursor is placed on top of an anodized aluminum oxide (AAO) membrane containing regular nanopore arrays, and slow heating under Ar ﬂow allows the molten polymer to wet the template through adhesive force. The polymer spread into the nanopores of the template to form polymer nanotubes. Upon carbonization the resulting multi-walled carbon nanotubes duplicate the nanopores morphology precisely. The process is demonstrated for 230, 50, and 20 nm pore membranes. The synthesized carbon nanotubes are characterized with scanning/transmission electron microscopies, Raman spectroscopy, and resistive measurements. Convenient functionalization of the nanotubes with this method