comparison between two ft-ir spectroscopy analytical procedures for micrograms determination of asbestos species in bulk materials比较两个微克傅立叶变换红外光谱分析方法确定石棉物种散装材料.pdfVIP

comparison between two ft-ir spectroscopy analytical procedures for micrograms determination of asbestos species in bulk materials比较两个微克傅立叶变换红外光谱分析方法确定石棉物种散装材料.pdf

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comparison between two ft-ir spectroscopy analytical procedures for micrograms determination of asbestos species in bulk materials比较两个微克傅立叶变换红外光谱分析方法确定石棉物种散装材料

American Journal of Analytical Chemistry , 2012, 3, 1-5 /10.4236/ajac.2012.31001 Published Online January 2012 (http://www.SciRP.org/journal/ajac) Comparison between Two FT-IR Spectroscopy Analytical Procedures for Micrograms Determination of Asbestos Species in Bulk Materials 1* 2 2 Luca De Stefano , Raffaele Cioffi , Francesco Colangelo 1Institute for Microelectronics and Microsystems, Unit of Naples, National Research Counsi, Napoli, Italy 2Technology Department, University of Naples “Parthenope”, Napoli, Italy * Email: luca.destefano@r.it Received October 14, 2011; revised November 18, 2011; accepted December 3, 2011 ABSTRACT The Fourier Transform Infrared (FT-IR) spectroscopy is by far known to be a useful technique for qualitative and quan- titative analysis of asbestos in bulk samples, since all asbestos species exhibit intense absorption peaks in the 4000 - 400 cm–1 region of the infrared spectrum. In the present work, we compare the accuracy and precision of two analytical procedures (the Linear Calibration Curve Method and the Method of Addition) for the quantitative determination of asbestos in a host matrix. We have found that, providing careful samples preparation, both techniques quantify the as- bestos content at the level of few micrograms with good precision. Due to less expensive equipment requirements and shorter analysis time, FT-IR can be a competitive analytical technique in the characterization of asbestos containing material with the respect to diffractometry or electron microscopy. Keywords:

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