continuous reaction crystallization of struvite in a dtm type crystallizer with jet pump of ascending suspension flow in a mixing chamber–kinetic approach of the process连续反应的鸟粪石结晶dtm型结晶器与喷射泵提升悬浮流混合chamber-kinetic过程的方法.pdfVIP

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continuous reaction crystallization of struvite in a dtm type crystallizer with jet pump of ascending suspension flow in a mixing chamber–kinetic approach of the process连续反应的鸟粪石结晶dtm型结晶器与喷射泵提升悬浮流混合chamber-kinetic过程的方法.pdf

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continuous reaction crystallization of struvite in a dtm type crystallizer with jet pump of ascending suspension flow in a mixing chamber–kinetic approach of the process连续反应的鸟粪石结晶dtm型结晶器与喷射泵提升悬浮流混合chamber-kinetic过程的方法

Journal of Crystallization Process and Technology, 2012, 2, 96-104 /10.4236/jcpt.2012.23012 Published Online July 2012 (http://www.SciRP.org/journal/jcpt) Continuous Reaction Crystallization of Struvite in a DTM Type Crystallizer with Jet Pump of Ascending Suspension Flow in a Mixing Chamber—Kinetic Approach of the Process 1 1 2 1 Agata Mazienczuk , Andrzej Matynia , Krzysztof Piotrowski , Boguslawa Wierzbowska 1Faculty of Chemistry, Wroclaw University of Technology, Wroclaw, Poland; 2Department of Chemical Process Engineering, Silesian University of Technology, Gliwice, Poland. Email: krzysztof.piotrowski@polsl.pl Received February 28th, 2012; revised April 2nd, 2012; accepted April 12th, 2012 ABSTRACT Reaction crystallization of struvite in water solutions containing 0.20 mass% of phosphate(V) ions by magnesium and ammonium ions addition was investigated experimentally. Process was carried out in DTM type crystallizer with liquid jet pump device in 298 K assuming stoichiometric conditions. Struvite crystals of mean size Lm 5.2 - 23.0 m were produced depending on pH (9 - 11) and mean residence time of suspension in a crystallizer  (900 - 3600 s). Under these conditions linear growth rate of struvite crystals (SIG MSMPR kinetic model) decreased 2-time with the increase in pH and 3-time with the elongation of mean residence time of crystal suspension from 7.11×10–9 m/s (pH 9,  900 s) –9 8 10 3 to 1.65 × 10 m/s (pH 11,  3600 s). Nucleation rate varied within the 7.9 × 10 - 1.8 × 10 1/(sm ) limits. Struvite product of maximal linear size exceeded 100 m with 10 vol% of 3 m fraction corresponded to pH 9 and  3600 s. Keywords: Struvite; Crystal Size Distribution (CS