原创力文档co-precipitation synthesis and characterization of nanocrystalline zinc oxide particles doped with cu2+ ions共同沉淀合成和表征纳米晶体掺杂氧化锌粒子cu2 +离子.pdfVIP
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co-precipitationsynthesisandcharacterizationofnanocrystallinezincoxideparticlesdopedwithcu2ions共同沉淀合成和表征纳米晶体掺杂氧化锌粒子cu2离子
Materials Sciences and Applications, 2012, 3, 543-551 543
/10.4236/msa.2012.38077 Published Online August 2012 (http://www.SciRP.org/journal/msa)
Co-Precipitation Synthesis and Characterization of
Nanocrystalline Zinc Oxide Particles Doped with
Cu2+ Ions
*
Mergoramadhayenty Mukhtar, Lusitra Munisa, Rosari Saleh
Departemen Fisika, FMIPA-Universitas Indonesia, Depok, Indonesia.
*
Email: rosari.saleh@ui.ac.id
Received May 8th, 2012; revised June 10th, 2012; accepted July 9th, 2012
ABSTRACT
Nanocrystalline Cu-doped ZnO particles were synthesized by the co-precipitation method. The composition, structural,
optical and magnetic characterizations were performed by energy dispersive X-Ray spectroscopy, X-Ray diffraction,
UV-Visible spectrometer, and vibrating sample magnetometer. The results confirmed that nanocrystalline Cu-doped
ZnO particles have a hexagonal wurtzite structure with a high degree of crystallization and a crystallite size of 10 - 16
nm. For Cu above 11 at%, the X-Ray diffraction pattern possessed CuO secondary phase which shows the solubility
limit of Cu in the ZnO lattice. Up to 11% at Cu, the presence of Cu in the ZnO lattice as Zn substitution indicated by an
in- crease in lattice parameter values. Nanoparticles showed weak ferromagnetic characteristics at room temperature.
The absence of secondary phase related to magnetic precipitate shown intrinsic ferromagnetic behaviour.
Keywords: Cu-Doped ZnO; Structural Properties; Room Temperature Ferromagnetism
1. Introduction while others claims that ferromagnetic ordering is in-
trinsic [9]. Motivated by these contradictory results, e
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