原创力文档crystal structure, thermal analysis and ir spectroscopic investigation of bis (n-methyl anilinium) sulfate晶体结构、热分析和红外光谱对bis(n-methyl anilinium)硫酸.pdfVIP
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crystal structure, thermal analysis and ir spectroscopic investigation of bis (n-methyl anilinium) sulfate晶体结构、热分析和红外光谱对bis(n-methyl anilinium)硫酸
Open Journal of Inorganic Chemistry, 2011, 1, 47-53 OJIC
doi:10.4236/ojic.2011.13007 Published Online October 2011 (http://www.SciRP.org/journal/ojic/).
Crystal structure, thermal analysis and IR spectroscopic
investigation of bis (N-methyl anilinium) sulfate
*
Taha Guerfel , Amor Jouini
Laboratoire de Chimie du Solide, Faculté des Sciences de Monastir, Monastir, Tunisie.
Email: taha_guerfel@yahoo.fr
Received 10 August 2011; revised 20 September 2011; accepted 10 October 2011.
ABSTRACT influencing the dimensions of sulfate anion–organic ca-
tion interaction. We report here the chemical preparation,
Chemical preparation, X-ray single crystal, thermal crystallographic features, thermal behavior, and IR ana-
analysis and IR spectroscopic investigation of (C7H10 lysis of a new organic sulfate, (C H N) ·SO .
7 10 2 4
N)2·SO4 denoted NMAS are described. The NMAS
2. EXPERIMENT
crystallizes in the triclinic system with P-1 space
group. Its unit cell dimensions are a = 9.6150(5) Å, b 2.1. Chemical Preparation
= 9.9744(3) Å, c = 10.2767(6) Å, = 68.069(3), =
62.929(2), = 67.285(3) with V = 785.72(7) Å3 and Z = Crystals of NMAS were prepared by slow evaporation at
2. The structure has been solved using direct me- room temperature of 400 mL of an aqueous solution of
thod and refined to a reliability R factor of 3.62%. H2SO4 (10–1 M), neutralized by 0.0
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