crystallization kinematics and dielectric behavior of (ba,sr)tio3 borosilicate glass ceramics结晶的运动学和介电行为(ba,sr)tio3硼硅玻璃陶瓷.pdfVIP

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crystallization kinematics and dielectric behavior of (ba,sr)tio3 borosilicate glass ceramics结晶的运动学和介电行为(ba,sr)tio3硼硅玻璃陶瓷.pdf

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crystallization kinematics and dielectric behavior of (ba,sr)tio3 borosilicate glass ceramics结晶的运动学和介电行为(ba,sr)tio3硼硅玻璃陶瓷

New Journal of Glass and Ceramics, 2012, 2, 126-131 /10.4236/njgc.2012.23018 Published Online July 2012 (http://www.SciRP.org/journal/njgc) Crystallization Kinematics and Dielectric Behavior of (Ba,Sr)TiO3 Borosilicate Glass Ceramics 1 1* 2 Avadhesh Kumar Yadav , Chandkiram Gautam , Prabhakar Singh 1Department of Physics, University of Lucknow, Lucknow, India; 2Department of Applied Physics, Institute of Technology, Banaras Hindu University, Varanasi, India. * Email: gautam_ceramic@ Received January 16th, 2012; revised March 24th, 2012; accepted April 27th, 2012 ABSTRACT Perovskite [(Ba Sr )TiO ]-[2SiO -B O ]-[K O]-La O glass was prepared by conventional melt quench method. The 0.6 0.4 3 2 2 3 2 2 3 differential thermal analysis (DTA) was performed on glass sample in the temperature range from 100˚C to 1000˚C by different heating rate to study the crystallization kinematics. The kinetic parameters characterizing the crystallization have been determined using an Arrhenius model. Glass samples were subjected to appropriate heat treatment schedules for their suitable crystallization. X-ray diffraction analysis (XRD) of glass and glass ceramic samples were done to check the amorphous state and crystalline nature. XRD of glass ceramic sample shows the major perovskite phase of BaTiO (BT) along with the formation of secondary phases Ba TiSi O (BTS) and Ba Ti B O (BTB). Scanning elec- 3 2 2 8 2 2 2 9 tron microscopy (SEM) is also studied to see the morphology of the grains of major and secondary phase formation in BST glass ceramic samples. La O is played an important role to increase the nucleation of the crystall