原创力文档difficulties in the use of ground bacterial cellulose (bc) as reinforcement of polylactid acid (pla) using melt-mixing and extrusion technologies困难的使用地面细菌纤维素(bc)强化polylactid酸(pla)使用melt-mixing和挤压技术.pdfVIP
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difficulties in the use of ground bacterial cellulose (bc) as reinforcement of polylactid acid (pla) using melt-mixing and extrusion technologies困难的使用地面细菌纤维素(bc)强化polylactid酸(pla)使用melt-mixing和挤压技术
Open Journal of Composite Materials, 2012, 2, 97-103 97
/10.4236/ojcm.2012.23011 Published Online July 2012 (http://www.SciRP.org/journal/ojcm)
Difficulties in the Use of Ground Bacterial Cellulose (BC)
as Reinforcement of Polylactid Acid (PLA) Using
Melt-Mixing and Extrusion Technologies
1 1 2 3
Katrin Ganß , Axel Nechwatal , Katrin Frankenfeld , Kerstin Schlufter
1Department of Textile and Material Research, Thueringisches Institut fuer Textil und Kunststoff-Forschung e.V., Rudolstadt,
Germany; 2Department Biotechnology, fzmb GmbH Forschungszentrum für Medizintechnik und Biotechnologie, Bad Langensalza,
Germany; 3Thueringer Landesamt fuer Lebensmittelsicherheit und Verbraucherschutz (TLLV), Bad Langensalza, Germany.
Email: ganss@titk.de
Received May 23rd, 2012; revised June 20th, 2012; accepted July 11th, 2012
ABSTRACT
Bacterial cellulose (BC) was ground to make the material suitable for compounding with polylactid acid (PLA). The
content of BC in PLA was changed between 5 and 20 wt%. By increasing the BC content of the composite DSC meas-
urements showed an increase of crystallinity (χ ). Annealing at 90˚C resulted in a further increase of χ . Analysis of the
c c
dynamic mechanical behavior showed a sharp decline of the storage module (G’) above the glass transition temperature
(Tg) while such a sharp decline did not occur for annealed samples. This indicates that the stiffness of PLA even above
Tg can be improved by BC and annealing.
Keywords: Polymer-Matrix Composite; Extrusion; Bacterial Cellulose
1. Introduction already pointed out the potentia
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