原创力文档e-beam graft polymerization of hydrophilic peg-methacrylate on the surface of pmma电子束表面接枝聚合的亲水性peg-methacrylate pmma.pdfVIP
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e-beam graft polymerization of hydrophilic peg-methacrylate on the surface of pmma电子束表面接枝聚合的亲水性peg-methacrylate pmma
Journal of Surface Engineered Materials and Advanced Technology, 2012, 2, 264-270
/10.4236/jsemat.2012.24040 Published Online October 2012 (http://www.SciRP.org/journal/jsemat)
E-Beam Graft Polymerization of Hydrophilic
PEG-Methacrylate on the Surface of PMMA
1 2*
Seong-Cheol Kim , PilHo Huh
1Department of Nano, Medical and Polymer Materials, Yeungnam Univeristy, Gyeongsan, Republic of Korea; 2Solar Energy RD
Center, Samsung Electronics Co., Ltd., Yongin, Republic of Korea.
*
Email: piro94@
Received July 23rd, 2012; revised August 29th, 2012; accepted September 9th, 2012
ABSTRACT
The graft polymerization of hydrophilic monomers on the surface of hydrophobic PMMA was performed using an elec-
tron beam (e-beam). The dose of e-beam irradiation, reaction concentration, temperature, and reaction time were used to
study the effect of variables on the graft density of poly (ethylene glycol)-methacrylate. The results demonstrated that
the weight percentage of graft polymer increased with increasing temperature, time and monomer concentration. How-
ever, the weight of the graft polymer did not increase with the increasing dose of e-beam irradiation. The change of the
contact angle of the water droplet on the PMMA surface was monitored as a function of a reaction time. The results
showed that the contact angle decreased up until a specific time and then leveled off to an approximately constant value
after a certain reaction time of the graft polymerization. Transmission electron microscopy proved that the constant
value of the contact angle was due to the local survival of surface radicals followed by the perpendicular diffusion of
monomers only into the bulk of the surface-modified area on the sheet surface.
Keywords: Electron Beam; Surface Graft; Contact Angle; ATR; TEM
1. Introduction cantly alter the s
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