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Hindawi Publishing Corporation International Journal of Photoenergy Volume 2012, Article ID 469178, 12 pages doi:10.1155/2012/469178 Research Article Sol-Gel-Hydrothermal Synthesis of the Heterostructured TiO /N-Bi WO Composite with High-Visible-Light- and 2 2 6 Ultraviolet-Light-Induced Photocatalytic Performances Jiang Zhang,1 Zheng-Hong Huang,1 Yong Xu,2 and Feiyu Kang1 1 Laboratory of Advanced Materials, Department of Materials Science and Engineering, Tsinghua University, Beijing 100084, China 2 Department of Technology, Beijing Tongfang Puri-Tech Co., Ltd., Beijing 100083, China Correspondence should be addressed to Zheng-Hong Huang, zhhuang@ and Feiyu Kang, fykang@ Received 15 July 2011; Accepted 22 August 2011 Academic Editor: Jinlong Zhang Copyright © 2012 Jiang Zhang et al. This is an open access article distributed under the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited. The heterostructured TiO /N-Bi WO composites were prepared by a facile sol-gel-hydrothermal method. The phase structures, 2 2 6 morphologies, and optical properties of the samples were characterized by using X-ray powder diffraction (XRD), scanning electron microscopy (SEM), high-resolution transmission electron microscopy (HRTEM), energy dispersive spectroscopy (EDS), and UV-vis diffuse reflectance spectroscopy. The photocatalytic activities for rhodamine B of the as-prepared products were measured under visible and ultraviolet light irradiation at room temperature. The TiO /N-Bi WO composites exhibited much