薄层扫描法测定喉咽舒中胆酸的含量（Determination of cholic acid in hypopharyngeal Shu by TLC）.docVIP

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薄层扫描法测定喉咽舒中胆酸的含量（Determination of cholic acid in hypopharyngeal Shu by TLC）.doc

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薄层扫描法测定喉咽舒中胆酸的含量（Determination of cholic acid in hypopharyngeal Shu by TLC）

薄层扫描法测定喉咽舒中胆酸的含量（Determination of cholic acid in hypopharyngeal Shu by TLC） Determination of cholic acid in hypopharyngeal Shu by TLC Update Date: 2010-06-08 Click: ever test sun Li Huixia! Abstract: the content of cholic acid in hypopharyngeal Shu particles were determined by TLC fluorescence scanning. The chromatographic conditions were as follows: 0.5%CMC-Na silica gel G plate, using chloroform ethyl acetate acetic acid (5: 5: 1), by spraying 30% sulfuric acid ethanol solution, drying at 105 DEG C about 5min color scanning wavelength is 365nm, the average recovery was 97.9%, RSD was 2.2%. The experiment shows that this method is simple, accurate and can be used for the quality control of the preparation. Keywords: @ hypopharyngeal Shu particles / chemical / chemical cholic acid; CLC number: R284.1, document identification code: A, article number: 1003-9783 (1999) 06-0372-02 Shu particles from hypopharyngeal hospital clinical prescription prescription. I plant for the development of new drugs. Mainly from honeysuckle, artificial bezoar and other four kinds of drugs, with Yin heat, phlegm, throat open sound effects. Among them, artificial bezoar is the main component, cholic acid is the main effective component of artificial bezoar. In order to control the quality of the granules effectively, the content of cholic acid was determined by TLC scanning method as the quality control index. 1 materials and methods 1.1 instrument and reagent CAMAG TLC Scanner - type III (Switzerland), quantitative capillary, CAMAG- TLC applicator, CAMAG double slot expansion cylinder, silica gel G (Qingdao marine plant), cholic acid (control China control of pharmaceutical and Biological Products Institute), experimental materials purchased from Guangzhou medicine company, with all reagents for the analysis of pure. Hypopharyngeal Shu particles for homemade, batch number 1.2 standard solution preparation of precision said cholic acid control 3mg into 10ml volumetric flask, add