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a new furostanol glycoside from tribulus terrestris一个新的从刺蒺藜furostanol糖苷.pdf

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a new furostanol glycoside from tribulus terrestris一个新的从刺蒺藜furostanol糖苷

Molecules 2010, 15, 613-618; doi:10.3390/molecule OPEN ACCESS molecules ISSN 1420-3049 /journal/molecules Communication A New Furostanol Glycoside from Tribulus terrestris Yajuan Xu 1,3, Yonghong Liu 4, Tunhai Xu 2,*, Shengxu Xie 1, Yunshan Si 1, Yue Liu 1, 1 2 1 Haiou Zhou , Tonghua Liu and Dongming Xu 1 Academy of Traditional Chinese Medicine of Jilin Province, Changchun 130021, China; E-Mail: xyj6492@ (Y.X.) 2 Department of Traditional Chinese Medicine Chemistry, School of Traditional Chinese Medicine, Beijing University of Chinese Medicine, Beijing 100102, China 3 Tianjin University of Traditional Chinese Medicine, Tianjin 300193, China 4 Key Laboratory of Marine Bio-resources Sustainable Utilization, South China Sea Institute of Oceanology, Chinese Academy of Sciences, No. 164 West Xingang Road, Guangzhou 510301, China; E-Mail: yonghongliu@ (Y.L.) * Author to whom correspondence should be addressed; E-Mail: thxu@ Received: 10 November 2009; in revised form: 13 January 2010 / Accepted: 18 January 2010 / Published: 27 January 2010 Abstract: Besides two known glycosides, a new furostanol glycoside was isolated from the Fruits of Tribulus terrestris L. The structure of the new furostanol glycoside was established as 26-O-β-D-glucopyranosyl-(25S)-5α-furostane-20(22)-en-12-one-3β, 26-diol- 3-O-α-L-rhamnopyranosyl-(1→2)-[β-D-glucopyranosyl-(1→4)]-β-D-galactopyranoside (1) on the basis of 1D and 2D-NMR techniques, in