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conductometric sensors for monitoring degradation of automotive engine oil电导传感器监测汽车机油的退化.pdf

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conductometric sensors for monitoring degradation of automotive engine oil电导传感器监测汽车机油的退化

Sensors 2011, 11, 8611-8625; doi:10.3390/s110908611 OPEN ACCESS sensors ISSN 1424-8220 /journal/sensors Article Conductometric Sensors for Monitoring Degradation of Automotive Engine Oil † Usman Latif and Franz L. Dickert * Department of Analytical Chemistry, University of Vienna, Waehringer Strasse 38, A-1090 Vienna, Austria; E-Mail: usman.latif@univie.ac.at * Author to whom correspondence should be addressed; E-Mail: Franz.Dickert@univie.ac.at. † Dedicated to Professor Dr. Adolf Neckel on the occasion of his 85th birthday. Received: 16 July 2011; in revised form: 31 August 2011 / Accepted: 1 September 2011 / Published: 5 September 2011 Abstract: Conductometric sensors have been fabricated by applying imprinted polymers as receptors for monitoring engine oil quality. Titania and silica layers are synthesized via the sol-gel technique and used as recognition materials for acidic components present in used lubricating oil. Thin-film gold electrodes forming an interdigitated structure are used as transducers to measure the conductance of polymer coatings. Optimization of layer composition is carried out by varying the precursors, e.g., dimethylaminopropyltrimethoxysilane (DMAPTMS), and aminopropyl-triethoxysilane (APTES). Characterization of these sensitive materials is performed by testing against oil oxidation products, e.g., carbonic acids. The