preparation and electrochemical characterization of a carbon ceramic electrode modified with ferrocenecarboxylic acid碳陶瓷电极的制备及电化学特性与ferrocenecarboxylic酸改性.pdfVIP

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preparation and electrochemical characterization of a carbon ceramic electrode modified with ferrocenecarboxylic acid碳陶瓷电极的制备及电化学特性与ferrocenecarboxylic酸改性.pdf

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preparation and electrochemical characterization of a carbon ceramic electrode modified with ferrocenecarboxylic acid碳陶瓷电极的制备及电化学特性与ferrocenecarboxylic酸改性

Sensors 2011, 11, 1361-1374; doi:10.3390/s110201361 OPEN ACCESS sensors ISSN 1424-8220 /journal/sensors Article Preparation and Electrochemical Characterization of a Carbon Ceramic Electrode Modified with Ferrocenecarboxylic Acid 1 1 2 1, Tatiane Skeika , Cristiane R. Zuconelli , Sergio T. Fujiwara and Christiana A. Pessoa * 1 Department of Chemistry, Universidade Estadual Ponta Grossa, Avenida Carlos Cavalcanti 4748, Uvaranas, Ponta Grossa, Brazil; E-Mails: tatiuepg@ (T.S.); criszuconelli@ (C.R.Z.) 2 Department of Chemistry, CEDETEG—Universidade Estadual do Centro-Oeste, Rua Presidente Zacarias 875, Guarapuava, Brazil; E-Mail: sergiofujiwara@.br (S.T.F.) * Author to whom correspondence should be addressed; E-Mail: christiana.pessoa@pq.br; Tel.: +55-42-322-037-31; Fax: +55-42-322-030-42. Received: 3 December 2010; in revised form: 4 January 2011 / Accepted: 17 January 2011 / Published: 25 January 2011 Abstract: The present paper describes the characterization of a carbon ceramic electrode modified with ferrocenecarboxylic acid (designated as CCE/Fc) by electrochemical techniques and its detection ability for dopamine. From cyclic voltammetric experiments, it was observed that the CCE/Fc presented a redox pair at Epa = 405 mV and Epc = 335 mV (ΔE = 70 mV), related to the ferrocene/ferrocenium process. Studies showed a considerably increase in the