原创力文档synthesis of 1-[(2-oxonaphthalen-1(2h)-ylidene)methyl]urea合成1 -[(2-oxonaphthalen-1(2 h)-ylidene)甲基]尿素.pdfVIP
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synthesis of 1-[(2-oxonaphthalen-1(2h)-ylidene)methyl]urea合成1 -[(2-oxonaphthalen-1(2 h)-ylidene)甲基]尿素
Molbank 2009, M595
OPEN ACCESS
molbank
ISSN 1422-8599
/journal/molbank
Short Note
Synthesis of 1-[(2-Oxonaphthalen-1(2H)-ylidene)methyl]urea
*
Jiehua Xu, Anjun Chen and Qingjian Liu
College of Chemistry, Chemical Engineering and Materials Science
Engineering Research Center of Pesticide and Medicine Intermediate Clean Production
Ministry of Education, Shandong Normal University, Jinan 250014, P. R. China
* Author to whom correspondence should be addressed; E-mail: liuqj@
Received: 7 January 2009 / Accepted: 13 March 2009 / Published: 18 March 2009
Abstract: An unexpected product, 1-[(2-oxonaphthalen-1(2H)-ylidene)methyl]urea 4 of
the condensation reaction of 2-hydroxy-1-naphthaldehyde with or without ethyl
benzoylacetate and urea under hydrochloric acid-catalyzed and solvent-free conditions is
reported.
Keywords: 1-[(2-Oxonaphthalen-1(2H)-ylidene)methyl]urea; Condensation reaction
Solvent-free conditions
Dihydropyrimidinones (DHPMs) have attracted considerable interest due to the promising
biological and pharmacological properties as calcium channel blockers, antihypertensive agents, and
anticancer drugs associated with this heterocyclic scaffold.1,2 Thus, the synthesis of such a heterocyclic
nucleus is of considerable importance, and quite a number of synthetic modifications based on the
Biginelli three-component condensation reaction of aldehyde, β-ketoes
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