某工厂污水化验综合测试步骤（Comprehensive test procedure of sewage test in a factory）.docVIP

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某工厂污水化验综合测试步骤（Comprehensive test procedure of sewage test in a factory）.doc

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某工厂污水化验综合测试步骤（Comprehensive test procedure of sewage test in a factory）

某工厂污水化验综合测试步骤（Comprehensive test procedure of sewage test in a factory） Chemical oxygen demand (COD) determination (daily measurement of blank sample, water sample and water sample)? Chemical oxygen demand: the amount of oxidant consumed in the treatment of water samples with potassium dichromate as the oxidant under the condition of strong acid and heating. The unit is mg/L. Potassium dichromate is used in our factory. ? (1) methods and principles: in a strongly acidic solution, a reduced amount of potassium dichromate was used to oxidize the reducing substance in aqueous solution. Excess potassium dichromate was used as an indicator, and ferrous ammonium sulfate was used as the indicator. The amount of oxygen consumed by the reducing substance in the water sample is calculated according to the dosage of ferrous ammonium sulfate. (two) determination procedures? 1. Take back the water sample and shake off the water sample. ?? 2. Take 3 taper bottles, numbered 0, 1 and 2, and add 6 beads of glass to 3 conical bottles. ?? 3, to the 0 conical flask with 20mL of distilled water (fat of pipettes); to the 1 conical flask with 5mL water sample (with a pipette, 5mL with water rinse pipette 3 times), and then add 15mL distilled water (fat of pipettes); to the 2 conical flask plus 20mL samples (with fat of pipette with water rinse pipette 3 times). ?? 4, to 3 conical bottles, respectively, add 10mL potassium dichromate non-standard liquid (using 10mL potassium dichromate non-standard liquid transfer tube, use potassium dichromate non-standard liquid wash pipette 3 times). ?? 5, the conical bottles are placed on the electronic furnace respectively, and then open the water pipe, the water filled with condensation tube (do not open too large, experience). ?? 6, from the top of the condenser tube to 3 conical bottles, respectively, with 30mL silver sulfate (using 25mL small amount of barrel), and then shake separately 3 conical bottles. ?? 7, plug in the electronic stove plug, st