活性炭经氯化改性后其表面化学性质的研究（Study on surface chemical properties of activated carbon modified by chlorination）.docVIP

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活性炭经氯化改性后其表面化学性质的研究（Study on surface chemical properties of activated carbon modified by chlorination）.doc

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活性炭经氯化改性后其表面化学性质的研究（Study on surface chemical properties of activated carbon modified by chlorination）

活性炭经氯化改性后其表面化学性质的研究（Study on surface chemical properties of activated carbon modified by chlorination） Study on surface chemical properties of activated carbon modified by chlorination Ye Pingwei [[2]], Luan Zhiqiang, [1], Zhang Jingchang, [2], Zhang Zhongliang, [1], Li Yan, [1], Ma Lan, [1] Beijing Research Institute of Chemical Defense Institute, Beijing 100083) Beijing University of Chemical Technology, Beijing, 100029) In order to study the anti-aging properties of activated carbon, the BN-09 granular activated carbon was modified by chlorination at different temperatures. The surface chemical properties of the basic carbon and the modified samples were analyzed by XPS and Boehm titration. The results show that the chloride modification did not make its surface acidity decrease, alkaline increase, nor the activated carbon surface oxygen content is reduced, thereby improving the anti aging performance; combined with the chlorine atom and the surface of the activated carbon mainly C-Cl covalent forms, followed by acyl halide groups COC1, C-Cl group content of 300 C chloride on the surface of the sample is highest. Keywords activated carbon; aging; chlorination; XPS; Boehm titration; Study, on, the, surface, chemical, properties, of, AC, chlorination, after YE, Ping-wei, LUAN, Zhi-qiang, ZhANG, Jing-chang, ZhANG, Zhong-liang, LI, Yan, Ma, Lan (Research, Institute, of, Chemical, Defence, Beijing, 100083) (Beijing, University, of, chemical, and, technology, Beijing, 100029) Abstract In order to study the aging performance of activated carbon, BN-09 grain activated carbon is modified at various chlorinated temperatures. And the surface chemical properties of the BN-09 and a serious of modified samples are analyzed with XPS and Boehm titration. The results show that both the acid characteristic and the surface oxygen content of AC after chlorination are higher than that of the BN-09 activated carbon. In addition, the C-Cl bond is the main combine form in the surface of