渗透汽化膜技术回收含水异丙醇的工业研究-河北科技大学学报.pdfVIP

32 2 Vol. 32, No . 2 20 11 4 Journal of Hebei University of Science and T echnolo y Apr . 20 11 : 2011) 1 1 1 2 1 王 晴, 李玉洲, 魏建红, 张淑菊, 盖素霞 ( 1. 石药集团河北中润制药有限公司, 河北石家庄 050041; 2. 石药集团河北宏源化工有限公司, 河 北石家庄 052 165) : 采用渗透汽化膜技术对头孢曲 钠生产过程中的异丙醇回收进行了实验, 并与原有的盐萃 取回收工艺进行了比较实验考察了渗透汽化膜的脱水分离性能, 并为工业设计提供基础性数据 结果表明, 含水量为15%( 质量分数, 下同) 的异丙醇经渗透汽化膜脱水后得到含水量 1% 的异丙 醇, 处理量为6 000 k / d该工艺具有低能耗低污染的优势, 可完全代替盐萃取工艺 : 渗透汽化膜技术; 异丙醇; 回收; 工业研究 : T Q051; X703 : A Industrial research on isopropanol recovery by pervaporation membrane technolo y 1 1 1 2 1 WANG Qin , LI Yuzhou , WEI Jianhon , ZHANG Shuju , GE Sux ia ( 1. H ebei Zhon run Pharmaceutical Company Limited, Shijiazhuan Pharmaceutical Group, Shijiazhuan Hebei 05004 1, Chi na; 2. H ebei Hon yuan Chemical Company Limited, Shijiazhuan Pharmaceutical Group, Shijiazhuan H ebei 052165, China) Abstract: The pervaporat ion membrane t echolo y w as adopted to recover isopropanol used in the production process of ceftri axone of CSPC, and it w as compared w ith the ori inal salt extraction process. The dehy dration performance of the pervapora t ion membrane w as tested t o provide basic data for industrial desi n. The result showed with isopropanol that w ater content of no more than 1% could be recovered from isopropanol w ith w ater content of 15% by the pervaporation membrane techolo y, and the handlin capacity is 6 000 k / d. For the superiority of low ener y consumption and low pollution, the pervaporation membrane process could be used to replace the salt extraction process. Key words: pervaporat ion membrane t echnolo y; isopropanol; recovery ; industrial research , , 1%( ,