地钱总黄酮提取的研究-林产化学与工业.pdfVIP

24 2 Vol.24 No.2 2004 6 Chemistry and Industry of Forest Products June 2004 1, 2 1 1 1* 朱 华 , 肖建波, 钟世安, 周春山 , 黄海滨 ( 1. 中南大学 化学化工学院, 湖南长沙410083; 2. 广西中医学院, 广西 南宁530001) ZHU H : ( Marchantiap olymorpha L.) , 5 L (4 ) , , 16 : 70 , 0. 5 h, 3 , 80%, 115, 1.90%,95.83% : ; ; :TQ91; Q949.351. 1; R284.2 :A :0253- 2417(2004)02- 0069- 04 STUDY N LEACHING AND PURIFYING METH D F FLAV NES FR M MARCHANTIA POLYMORPHA L. 1,2 1 1 1 ZHU Hua , XIA Jian-bo , ZH NG Sh-i an , ZH U Chun-shan , HUANG Ha-i bing (1. College of Chemistry and Chemical ngineering, Central South University, Changsha 410083, China; 2. Guangxi Chinese Medical University, Nanning 530001, China) Abstract : The optimum technology of extracting flavones in Marchantiapolymorpha L.was studiedby orthogonaltest.Anor- 5 thogonal test tableL ( 4 ) was usedwith thefactors of extracting time,temperature,number of extraction times,ethanol con- 16 centration and ratio of solid-to-liquid.The content of flavoneswas determined by spectrophotometry.The optimum technology was:temperature 70 ,time 0.5 h,three times of extraction,80% Et H as extracting solvent, stock ratio 115.The extraction yield is 1.90%,and its purification about 95.83% with this method. Key words: Marchantiap olymorpha L.; flavones; orthogonal test (Marchantiapolymorpha L.) , , , , 3 000 , 1. 8%, , , , , ,,,, , ,, :2003- 11- 24 : ( 1960- ) , ,,, , *