果汁中胭脂红柠檬黄和日落黄含量检测能力验证研究.pdfVIP

第8 卷 第8 期 食品安全质量检测学报 Vol. 8 No. 8 2017 年8 月 Journal of Food Safety and Quality Aug. , 2017 果汁中胭脂红、柠檬黄和日落黄含量检测能力 验证研究 * 张 宁 , 钱沛泽, 牛承辉 (辽宁出入境检验检疫局, 大连 116001) 摘 要: 目的 通过分析、评定实验室的检测结果, 了解国内实验室对果汁中胭脂红、柠檬黄和日落黄的检 测能力。方法 采用果汁添加标准品的方式制备样品, 通过F 检验、Ss ≤0.3和| x y | ≤0.3法对所制备的样 品进行均匀性和稳定性检验。以稳健分析算法A 得出的稳健平均值和稳健标准差, 作为本次能力验证计划的 指定值和能力评定标准差, 利用 z 比分数进行参加实验室的能力评定。结果 参加实验室检测胭脂红、柠檬 黄和日落黄能力评定的满意率分别为79%、87%和77%。结论 大部分参加实验室对胭脂红、柠檬黄和日落 黄具备较好的检测能力。 关键词: 能力验证; 胭脂红; 柠檬黄; 日落黄 Proficiency testing of determination of carmine, tartrazine and sunset yellow in fruit juice * ZHANG Ning , QIAN Pei-Ze, NIU Cheng-Hui (Liaoning Entry-Exit Inspection and Quarantine Bureau, Dalian 116001, China) ABSTRACT: Objective To investigate the determination ability of carmine, tartrazine and sunset yellow of domestic laboratories by the analysis and evaluation of the test results. Methods The samples were prepared by adding standard material into fruit juice. The homogeneity and stability of samples were determined by F-test, Ss ≤0.3 and | x y | ≤0.3. The robust mean and robust standard deviation were calculated by arithmetic A of robust analysis and designated as the assigned value and ability evaluation standard deviation. The abilit