超临界co2萃取红花大金元烟叶净油工艺的优化及挥发性成分分析 optimization of supercritical co2 extraction conditions for honghuadajinyuan tobacco essence and analysis of its volatile components.pdfVIP

烟草科技／T0bacco science＆Technology烟草化学／TobaccoChemiBtry 超临界C02萃取红花大金元烟叶净油工艺的 优化及挥发性成分分析 念小魁，刘煜字‘．李学杉，郑琳，端李祥，王松峰 云南瑞升烟草技术(集团)有限公司，昆明高新开发区科医路4l号650106 关键词：红花大金元(红大)；烟叶；净油；超临界C0，萃取；正交试验；挥发性成分；气相色谱一质谱法 摘要：为优化红大烟叶净油的超临界CO：萃取工艺条件，采用L。(34)正交试验法对红大烟叶净油的提 取率进行了考察，并对其进行了气相色谱一质谱鉴定。结果表明：最佳萃取条件为萃取压力30MPa，萃 取温度45℃，C0：流量25kg／h，萃取时间2．0h；共鉴定出36种化学成分，其中含量较高的成分主要有 (2．00％)等。该净油能提升烟草本身香气，使烟香丰满飘逸，并能赋予卷烟独特的风格特征，可明显增 加卷烟的抽吸品质。优选得到的工艺可提高红大烟叶净油提取率，工艺稳定、可行。 中图分类号：TS411．1文献标识码：B文章编号：1002一086l(2011)04—0036—05 of ExtractionConditionsfbr TobaccoE鹞enceand Optimization SupercriticaIC02 Honghuadajinyuan ofitsVoIa蝴e AnaIysis Components NIAN WANGSONG—FENG XIAO—KUI，LIUYU—YU，LIXUE—SHAN，ZHENGLIN。DUANLI—XIANG，and 1 YunnanReascendTobacco 650 Technology(Group)Co．，Ltd．，Kunming06，China Keywords：Honghuadajinyuan；Tobaccole“；Essence；SupercriticalC02extraction；OrthogonaIexperiment； Volatile component；GC／MS orderto Abstract：In the ext瑚Lctionconditionsfor tobacco optimizesupellcriticalC02 Hongda e8sence，tlIe extractionwas thevolatile intheobtained yield inVestigatedbyL9(34)orthogonalexpe“ment，andcomponents extractswere theessencewas into asanaVor．Theresultsofthe analyzedbyGC／MS，and appliedcigal．ette indicatedthatthe extmction r8teandtimewere30 now experiments optimal pressure，temperature，C02 MPa， and2．0 were themainvolatile 45℃，25kg／h hours，Iespectively． identified，and Thirty·sixcomponents components