【精选】Characterization and activity in dry reforming of methane on NiMg-Al and Ni-MgO catalysts.pdf

【精选】Characterization and activity in dry reforming of methane on NiMg-Al and Ni-MgO catalysts.pdf

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【精选】Characterization and activity in dry reforming of methane on NiMg-Al and Ni-MgO catalysts

Catalysis Today 113 (2006) 194–200 /locate/cattod Characterization and activity in dry reforming of methane on NiMg/Al and Ni/MgO catalysts A. Djaidja a,b,*, S. Libs b, A. Kiennemann b, A. Barama a a ´ Laboratoire de Chimie du Gaz Nnaturel, Faculte de Chimie, USTHB BP.32.El-Alia, 16111 Bab-Ezzouar, Alger, Algeria b ECPM-LMSPC UMR CNRS 7515 25, Rue Becquerel, 67087 Strasbourg, France Available online 6 January 2006 Abstract Dry reforming of methane has been investigated on two series of catalysts either prepared by co-precipitation: n(Ni Mg )/Al, Ni Mg and x y x y NixAly or prepared by impregnation: Ni/MgO (mol% Ni = 5, 10). The catalysts, calcined at 600–900 8C, were characterized by different techniques: BET, H2-TPR, TPO, XRD, IR, and TEM-EDX analysis. The surface BET (30–182 m2 g1) decreased with increasing the temperature of calcination, after reduction and in the presence of Mg element. The XRD analysis showed, for n(Ni Mg )/Al catalysts, the presence of NiAl O x y 2 4 and NiO–MgO solid solutions. The catalyst reducibility decreased with increasing the temperature of pretreatment. The n(Ni Mg )/Al catalysts

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