无蔗糖冷冻饮品中蔗糖的测定-食品安全质量检测学报.pdfVIP

6 10 Vol. 6 No. 10 2015 10 Journal of Food Safety and Quality Oct. , 2015 * 张 宇, 张良政, 程国栋, 吴方舟, 李晓丹, 吴小慧 , 金 珠 ((), 243000) 摘 要: 目的 方法 , -结果 2 0.1~0.5 g/L r 0.99, g/100 g , 93.5%~99.5%, 1.8%~3.4%结论 , , 关键词: ; ; Determination of sucrose in sucrose-free frozen drinks ZHANG Yu, ZHANG Liang-Zheng, CHENG Guo-Dong, * WU Fang-Zhou, LI Xiao-Dan, WU Xiao-Hui , JIN Zhu (Mengniu Dairy (Ma’anshan) Co. , Ltd., Ma’anshan 243000, China) ABSTRACT: Objective To establish a method for the determination of the sucrose in sucrose-free frozen drinks by ultra performance liquid chromatography evaporative light scattering detector(UPLC-ELSD). Methods The sucrose in sucrose-free frozen drinks samples was extracted with acetonitrile, centrifuged to precipitate impurities and then detected with UPLC-ELSD. Results The calibration curve for sucrose had a good linearity correlation in the concentration range of 0.1 g/L~0.5 g/L(r20.99). The recoveries at level of 0.2, 0.4, and 1.0 g/100 g fortified samples were ranged from 93.5% to 99.5%, with relative standard deviation of 1.8 %~3.4 %. Conclusion The method is simple, rapid, and accurate, and its performance can meet the requirements of the domestic and international legislation. It is s