54.消失模铸造制备镁合金表面复合层研究.pdfVIP

2010 中国铸造活动周论文集 ∗ 消失模铸造制备镁合金表面复合层研究 陈东风，董选普，樊自田， 马 戎 （华中科技大学材料成形与模具技术国家重点实验室，湖北 武汉 430074） 摘要：采用消失模铸造工艺，进行了镁合金表面制备合金化/陶瓷化复合层研究。选用金属铝粉作为合金 化主要元素，PbO-ZnO-Na2O 系低温玻璃粉为制备陶瓷涂层的主要材料。不同浓度的聚乙烯醇溶液分别用来 配制合金化和陶瓷化涂料。在真空度为－0.06MPa，温度为 800℃条件下浇注，在基体的表面形成了一定厚 度合金化/陶瓷化复合层。扫描电镜、线扫描分析、能谱分析用于研究复合层的微观组织结构和成分分布。 与单一的表面陶瓷化相比，表面的陶瓷层和合金化层形成良好的结合界面。显微硬度测试表明，从表面至 基体复合层的硬度成梯状分布，硬度值的变化与单一的陶瓷层相比有一个过渡区，这有利于提高表面陶瓷 层与基体的界面结合质量。 关键词：消失模铸造；镁合金；复合层；结合界面；显微硬度 Research on Mg-alloy Surface Composite Layer Prepared by Lost Foam Casting Technology Chen Dong-feng，Dong Xuan-pu ，Fan Zi-tian ，Ma rong (State Key Laboratory of Material Processing and Die Mold Technology，Huazhong University of Science and Technology，Wuhan 430074 China) Abstract: Evaporated pattern casting (EPC) process has been employed in the investigation of preparing alloying/ceramic composite layer on the Mg-alloy surface. Metal aluminum powder was chosen as the alloying element, PbO-ZnO-Na2O system low melting point glass powder was used as the material to prepare ceramic coating. The alloying/ceramic composite layer with a certain thickness was attained when the vacuum degree was -0.06MPa, pouring temperature was 800 ℃. Scanning electron microscopy (SEM), line composition scanning and energy dispersive X-ray spectrometer (EDS) were used to analyze the microstructure and composition distribution of composite layer. It has been found that a high quality bonding interface was formed between the alloying layer and surface ceramic coating, compared with the single surface ceramic coating. The hardness test shows that the micro-ha