枸杞总黄酮微波辅助提取工艺的优化.pdfVIP

ofAnhui 安徽农业科学。JoumM A鲥．Sci．2012．40(121：7377—7379 责任编辑石金友责任校对卢瑶 枸杞总黄酮微波辅助提取工艺的优化 750021) 孙波，王琨，郝鹏程，马润琴，马春兰，宋平 (宁夏大学生命科学学院，宁夏银JIl 摘要[目的]优化微波辅助提取枸杞中总黄酮的提取工艺。[方法]以芦丁为对照品，采用单因素试验和正交试验时影响枸杞总黄酮 提取得率的因素进行了考察，并优选最佳提取工艺。[结果]最佳提取工艺为：乙醇浓度为70％，料液比为l：30(∥m1)，微波辐射功率为 400W．辐射温度为120℃，提取时间为8 min；在此条件下．枸杞总黄酮的含量为18．3mg／g。[结论]与传统工艺相比，微波辅助提取枸 杞总黄酮具有高效、易于操作等优点。 关键词枸杞；总黄酮；微波辅助；正交试验 中图分类号$567．9；R284．2文献标识码A 文章编号0517—6611(2012)12—07377—03 ofMjclowave·assistedExtraction FIavonoidsFRUCTUSLYCⅡ Optimization TechnologyofTotal from SUNBoetal ofLife (CollegeScience，NingxiaUniversity．Yinehuan。Ningxia750021) Abstract microwave—assistedextraction oftotalflavonoidsfromFRucTUs [Ohjective]Tooptimize technology LYCn．fMethodl Using tinaBreferenee factorsthalinllueneed substance．Ihe microwave—assistedextractionofIotalfinvonoidswere meansof optimizedby single— factortestand ResultThe Wasas oflhogonaltest．f extractionoftotalflavonoids ethanolsolu． design optimal process follows：70％aqueous ratio1：30 duration8 120℃．Inthis tion，solid-liquidg／ml，extractingmin，microwavepower400 temperature condition。the W，extracting oftotalflavonoidswas18．3 withthetraditional extractionismoreeffi． yield rn∥g．IConclusionICompared technology，microwave—assisted mom totalflavonoidsfromFRUCTUS eienland easy—operating；nextracting LYCII． wordsFRUCTUSLYCII；Totalflavonnids；Miemwave．assisted；Orthogonaldesign Key