板蓝根化学成分研究ⅰ.pdfVIP

Chinese T r aditio na and Her ba D rugs 200 1 32 12 1057 ( ) 1 2 1 2 刘云海, 秦国伟 , 丁水平, 吴晓云 ( 1. , 4 30030; 2. , 2000 31) : 95% , , , , 2 , ( isaindig ot idione, ) , ( E ) -( E ) -3-( 3 , 5 -dimethox y -4 -hy dr ox y - ) -2- , 2 benzy idene indo ino ne : ; ; ; ( E ) - : R 284. 1: A : 0253 2670 ( 2001) 12 1057 04 Studies on chemical constituents from root of Isatis indig otica 1 2 1 2 LIU Y un-hai , QIN Guo -wei , DIN G Shui-ping , WU Xiao -y un ( 1. Af i iated T o ngj i Ho spit a of T o ngji M edica Co eg e, Huazhong U niv ersit y of Science and T echno o gy , Wuhan Hubei 4 300 30 , China; 2. Shang ha i Institute o f M ater ia M edica, Chinese A cademy of Sciences, Shanghai 2000 31, China) Abstract: ObjectT o ex t ract and separat e t he chemica constit uent s f rom t he ro ot of I satis ind ig otic a Fo rt . ( Crucif er ae ) . MethodsT he roo t of I . ind ig ot ica was perco at ed w it h 95% et hy a coho , part i- tio ned in so v ent s of diff erent po arities and f ina y iso at ed on si ica ge and macr opo rou s resin co um ns . T he purified compounds obt ained w ere ident ified and str uctura y e ucidated by t heir physicochemica pro p- er ties and spect ra ana y sis . ResultsT w o compounds w ere obtained and named as isaindigot idione ( ) and ( E ) -3-( 3 , 5 -dim et hox y-4 -hy dro xy benzy idene ) -2-indo ino ne. Conclusion T he t w o co mpounds w er e new . Key words: t he roo t o f I satis ind ig otic a Fo rt . ; ext ract ion and separat ion ; isaindigot idione; ( E ) -3-(