酚醛树脂废水COD测定方法研究.docVIP

本科毕业设计（论文） 题目 酚醛树脂废水COD测定方法研究 院 ( 系 ) 资源环境学院 专业名称 环境工程 年级班级 环境07-2班 学生姓名 指导教师 2011年 6月 10日 摘 要 化学需氧量（COD）是综合评价水体污染程度的重要指标，也是水质监测的一个重要项目。本文主要是运用三种不同的实验方法（标准法、密封法、微波法）准确测定酚醛树脂废水COD值,通过测定的数据对比和分析找出各自的优缺点，并根据实际水质情况及实验条件改进优化COD的测定方法步骤，以达到准确、安全、环保的要求，同时减少药品消耗、能源消耗、环境污染。实验过程采用并设计正交实验方法进行取样试验，确定密封法的最佳实验方案，并对微波法的最佳测定条件进行了探索研究，实验的目的主要是尽量降低COD测定成本。通过不同实验方法测定和分析发现，标准法测定结果准确可靠，但测定周期长， 一次回流需要2h,在药剂、水、电等方面消耗大，且易造成二次污染；密封法与标准法对比，测定结果相对准确，测定时间缩短66.7%，一次测定分析药剂使用量降低约4倍，大批水样测定成本更低，是一种很好的测定方法；微波法测定结果准确度及药剂消耗方面都介于标准法和密封法之间，测定时间最短，大概需要10分钟，并适用多个水样的测定，是一种不错的测定方法。 关键词：化学需氧量 ；酚醛树脂废水；标准法； 恒温箱密封法； 微波密封法 Abstract Chemical oxygen demand (COD) is a comprehensive evaluation of the degree of water pollution an important indicator of water quality monitoring is an important project. This paper is the use of three different experimental methods (standard method, sealed, microwave) accurate determination of phenolic resin wastewater COD value, comparing the measured data and analysis to identify the advantages and disadvantages, and according to the actual water quality and experimental conditions Improved Optimization Method for determination of COD steps to achieve accurate, safe and environmental requirements, while reducing drugs consumption, energy consumption, environmental pollution. Orthogonal experiment design of experimental methods used and sampling tests to determine the optimal experimental scheme sealing method, and microwave measurement conditions were the best exploration and research, the main purpose of the experiment is to minimize the cost of COD determination. Measured by different experimental methods and analysis, the standard method is accurate and reliable, but the determination of a long cycle, Need for a return 2h, in the pharmaceutical, water, electricity and so on consumption, but also lead to secondary pollution; sealing method compared with the standard method to determine the