年处理18万吨粗苯加氢精制工艺设计毕业论文绝对精品.doc

唐 山 学 院 毕 业 设 计 设计题目：年处理18万吨粗苯加氢精制工艺设计 系 别： 环境与化学工程系 班 级： 09石油化工生产技术（）18万吨/年粗苯加氢精制工艺设计 摘要 粗苯为中间体产品仅作为溶剂使用，但是精制后的焦化苯、焦化甲苯、焦化二甲苯等产品，是有机化工、医药和农药等的重要原料业内专家认为，粗苯加氢精制技术代表了粗苯加工精制的发展方向，这一技术在我国的推广使用，不仅可使宝贵的苯资源得到充分利用，还可有效改善粗苯精制的面貌，提高清洁生产的水平。在加氢工艺中，低温加氢工艺的加氢温度、压力较低，产品质量好，已被广泛用于石油重整油、高温裂解汽油、焦化粗苯为原料的加氢生产中，因此粗苯精制采用低温加氢精制工艺。苯甲苯Process Design of Hydrogenation of Crude Benzene with Annual Handling Capacity of 180 Thousand Tons Abstract Crude Benzol for intermediate products, only use as a solvent, but after refining coking benzene, coke toluene, xylene and other coking products, organic chemicals, pharmaceuticals and pesticides, such as the important raw materials, Industry experts believe that crude benzene hydrogenation technology for refining crude benzene represents the direction of development of this technology in China to promote the use of benzene is not only valuable resources can be fully utilized, can effectively improve the appearance of refined crude benzene, improve hygieneThe middle level. During the design process of hydrogenation, the hydrogenation of low-temperature hydrogenation process temperature, low pressure, product quality, has been widely used in the oil re-oil, high temperature pyrolysis gasoline, coking crude benzene hydrogenation for the production of raw materials, so the use of low-temperature crude benzene hydrogenation refining process. Accuracy of 99.9% pure benzene than toluene are more than 99% purity of product are better than other methods. Key words: Crude Benzene; hydrogenation; benzene; Toluene; process design 目录 1 引言 1 1.1设计的意义 1 1.2设计指导思想和原则 1 1.3设计依据 2 2 生产方法和工艺流程的确定 3 2.1工艺技术的比较与选择 3 2.1.1主要生产工艺技术简介 3 2.1.2工艺技术的比较与选择 4 2.2生产流程叙述 4 3 物料衡算 6 3.1原料粗苯计算 6 3.2两苯塔进出料 6 3.3预精馏塔进出料 6 3.4纯苯塔进出料 6 4 设备的计算与选型 7 4.1塔体的工艺计算： 7 4.1.1精馏塔的物料衡算 7 4.1.2精馏塔塔顶、塔底、进料板温度计算 8 4.1.3精馏塔塔顶、塔底、进料板密度流量的计算 15 4.1.4最小回流比、回流比及操作线的计算 16 4.1.5塔板的计算 18 4.1.6表面张力的计算 19 4.1.7液相平均黏度 20 4.1.8塔径的计算 21 4.2 塔板尺寸的设