毕业设计（论文）-流动注射分光光度法测定水样中高锰酸盐指数精选.docx

流动注射分光光度法测定水样中高锰酸盐指数目录摘要IAbstractII引言1第1章绪论21.1水质21.2高锰酸盐指数的研究21.2.1高锰酸盐指数21.2.2高锰酸盐指数的测定方法21.2.3高锰酸盐指数测定方法的发展方向41.3流动注射分析法51.3.1流动注射分析原理51.3.2流动注射分析特点51.3.3流动注射法的应用51.3.4流动注射发展趋势6第2章实验部分82.1仪器与试剂82.1.1主要仪器82.1.2主要试剂82.1.3试剂的配制82.2方法原理和适用范围92.2.1BDFIA-8000工作原理92.2.2应用范围92.3分析前准备工作92.3.1仪器的检测92.3.2仪器的设定92.3.3标液的配制102.4实验步骤102.4.1准备仪器102.4.2取样102.4.3样品测定11第3章结果与分析123.1标准样及部分水样测量值123.2标准曲线143.3检出限153.4精密度与准确度163.5加标回收率183.6流动注射分光光度法与国标酸性高锰酸钾法对比18结论21致谢22参考文献23流动注射分光光度法测定水样中高锰酸盐指数摘要：本文对高锰酸盐指数的测定方法进行了简单介绍，主要研究了流动注射分光光度法对水样中高锰酸盐指数的测定。使用新一代全自动流动注射高锰酸盐指数分析仪，对部分生活水样进行测定分析，对其检出限，精密度，准确度和加标回收率等进行测定。标准曲线回归方程为C=0.1444*A-0.0209，R2=0.9936，检出限为0.01mg/L，RSD=0.4%，加标回收率为91.0%~105.5%，最后与国家标准法酸性高锰酸钾法进行对比实验。结果表明流动注射分光光度法既具有分光光度法选择性强、灵敏度高、抗干扰能力强的特点，还有流动注射分析方法自动快速、操作简单等优势，对水样中高锰酸盐指数测定有检出限低，精密度高，准确度好等优势。说明流动注射法能够满足各监测部门对水样的检测要求，在水质分析在线检测领域具有良好的前景。关键词：高锰酸盐指数分光光度法流动注射Determination of Permanganate Index in Water by Flow Injection SpectrophotometryAbstract：In this paper, the determination method of permanganate index is briefly introduced, and the determination of permanganate index in water sample by flow injection spectrophotometry. A new generation of automatic flow injection of permanganate index analyzer was used to determine the detection limits of some living water samples, and their detection limits, precision, accuracy and spiked recovery were measured. The regression equation was C=0.1444*A-0.0209, R2=0.9936, the detection limit was 0.01mg/L, RSD=0.4%, the recoveries were 91.0% ~ 105.5%, and finally with the national standard method acid potassium method for comparative experiments. The results show that the flow injection spectrophotometry not only has the characteristics of selective spectrophotometry, high sensitivity and strong anti-interference ability, as well as the advantages of rapid and simple method of flow injection analysis, and the determination of permanganate index in water samples Detection limit is low, high precision, good accuracy and other advantages. It shows tha