利用废玻璃和粉煤灰制备建筑微晶玻璃及其性能分析-preparation and performance analysis of building glass-ceramics from waste glass and fly ash.docxVIP

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利用废玻璃和粉煤灰制备建筑微晶玻璃及其性能分析-preparation and performance analysis of building glass-ceramics from waste glass and fly ash.docx

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利用废玻璃和粉煤灰制备建筑微晶玻璃及其性能分析-preparation and performance analysis of building glass-ceramics from waste glass and fly ash

present rapid sintering rate, more densification and higher degree of crystallization. The bending strength of glass-ceramics from fine powder is increased by more than 55%. The addition of 10% MgO achieves the best performance of augite-forsteriteglass- ceramics sintered at 1000 ℃ for 2 h, with a volume density of 1.94 g/cm3, abending strength of 78 MPa, and a crystallization degree of 62%. The addition of 15% clay achieves the best performance of augite-anorthite glass-ceramics sinteredat 1000 ℃ for 2 h, with a volume density of 2.3 g/cm3, a bending strength of 90MPa, and a crystallization degree of 48%. Hence, for the three crystallization promoters the addition of clay has the best effect on the densification and bending strength of glass-ceramics.Using waste glass, flyash and clay as raw materials, the heating rate in the sintering process was studied to clarify its effect on the structure and properties ofglass-ceramics. Compared to the conventional sintering with 10 ℃/ min, two rapidsintering processes including 30 ℃/min and the direct insertion of samples at the sintering temperature present significantly reduced sintering activation energies. Forrapid sintering, the glass-ceramics have higher volume density, smaller pore size，more complete crystallization and higher strength. The sintering temperature is decreased, and the maximum bending strength of 107 MPa is obtained when theglass-ceramic was directly inserted at 950 ℃. Finally, several colorants were appliedto prepared colorful glass-ceramics with different decorative appearances.Keywords: waste glass, fly ash, construction glass-ceramics, direct powder sintering, rapid sintering目录第 1 章绪论 ..................................................... 11.1 引言 ...................................................... 11.2 建筑微晶玻璃简介 .......................................... 21.2.1 建筑微晶玻璃发展现状 ............................... 21.2.2 固体废弃物在建筑微晶玻璃中的应用 ................... 31.3 建筑微晶玻璃制备工艺 .......................