可再分散聚合物粉末的制备分析-preparation and analysis of redispersible polymer powder.docxVIP

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可再分散聚合物粉末的制备分析-preparation and analysis of redispersible polymer powder.docx

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可再分散聚合物粉末的制备分析-preparation and analysis of redispersible polymer powder

The modified PVAc emulsion was gained by VAc emulsion copolymerizing with VeoVa10, which had excellent water-resistance and base-resistance. The optimum conditions of copolymerization as follow: the solid content is 45.0~50.0%; 5.0~10.0% (the weight ratio to main monomer) VeoVa10 as modified monomer; PVA-1788 as protective colloid and its dosage is 7.5~15.0% (the weight ratio to monomer); the compound of OP-10 and SDS as the emulsification agent, the weight ratio is about 2:1, its dosage to monomer is 3.0~4.0%; 0.4~0.5% (NH4)2S2O8 as initiator; the buffer agent, dispersant and other assistant agents were added appropriately. Thepolymerization was carried out at 75~85 ℃, the rate of monomer feeding wascontrolled in 3.0~4.0 h.Chapter Four: Preparation of poly (vinyl acetate) emulsion modified with acrylic acid and butyl acrylateThe modified PVAc emulsion was prepared by VAc emulsion copolymerizing with AA and BA, which had excellent water-resistance, base-resistance, and lower cost. The optimum conditions of copolymerization as follow: the solid content is 45.0~50.0%; 3.0~4.0% (the weight ratio to main monomer) AA as modified monomer; 5.0~10.0% (the weight ratio to main monomer) BA as modified monomer;PVA-1788 as protective colloid and its dosage is 7.5~15.0% (the weight ratio to monomer); the compound of OP-10 and SDS as the emulsification agent, the weight ratio is about 2:1, its dosage to monomer is 3.0~4.0%; 0.4~0.5% (NH4)2S2O8 as initiator; the buffer agent, dispersant and other assistant agents were added appropriately. Thepolymerization was carried out at 75~85 ℃, the rate of monomer feeding wascontrolled in 3.0~4.0 h.Chapter Five: Preparation of several redispersible polymer powders by spray dryingIn the thesis, three kinds of self-prepared emulsions were used as matrix-latexes. And drying equipment was DC-1500 model experimental spray drier. Three kinds of RPP products which had excellent performance were prepared by