差示扫描量热法测定化学对照品纯度的应用分析-application analysis of differential scanning calorimetry in determining the purity of chemical reference substance.docxVIP
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差示扫描量热法测定化学对照品纯度的应用分析-application analysis of differential scanning calorimetry in determining the purity of chemical reference substance
AbstractChemicalreferencesubstancesplayanimportantroleindrugqualitycontrol,whichiswidelyusedforqualitativeandquantitativeanalysisofchemicaldrugs.Thepurityvaluesofchemicalreferencesubstancesproposedforassaymustbeaccurateastheyareusedforthetransferofthemeasurementvalue.Asaguidingprinciple,purityof99.5%orhigherisdesirable,calculatedonthebasisofthematerialinitsanhydrousformorfreeofvolatilesubstances.Inthecalibrationprocessofchemicalreferencestandard,themassbalancemethodisrecommended.Inthisstudy,theDSCmethodwasusedandevaluatedscientificallybycomparingtheresultanduncertaintywiththatofthemassbalancem
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