化工毕业设计--年产八万吨合成氨合成工段的设计.docVIP

目 录 摘要 1 关键词 1 1.前言 2 2.流程方案的确定 4 2.1生产原理 4 2.2各生产方法的特点 5 2.3工艺流程的选择 5 4.设计条件 7 5. 物料衡算 8 5.1 合成塔物料衡算 8 5.2氨分离器气液平衡计算 9 5.3冷交换器气液平衡计算 10 5.4 液氨贮槽气液平衡计算 11 5.5液氨贮槽物料计算 13 5.6合成系统物料计算 14 6 热量衡算 24 6.1冷交换器热量衡算 24 6.2氨冷器热量计算 26 6.3 循环机热量计算 27 6.4 合成塔热量计算 29 6.5 废热锅炉热量计算 30 6.6 热交换器热量计算 31 6.7 水冷器热量计算 32 6.8 氨分离器热量核算 33 7.主要设备选型 33 8.结语 37 参考文献 38 致谢.....................................................................................................................................39 摘要：氨合成工艺流程一般包括分离和再循环、氨的合成、惰性气体排放等基本步骤，上述基本步骤组合成为氨合成循环反应的工艺流程。其中氨合成工段是合成氨工艺的中心环节。新鲜原料气的摩尔分数组成如下：H2 74.5%，N2 24%，CH4 1.2%,Ar 0.3%，合成塔入口气的组成为NH3(2.5%),CH4+Ar(17%),要求合成塔出口气中氨的摩尔分数达到13.2%。通过查阅相关文献和资料，进行年产八万吨合成氨合成工段的设计，对该工艺流程进行了物料衡算、能量衡算，以及设备计算和选型。最后借助CAD技术绘制了该工艺流程图和换热器设备图。 关 键 词：氨合成 物料衡算 能量衡算 Abstract: There are ?many types of Ammonia synthesis technology and process, Generally,they includes ammonia synthesis, separation and recycling, inert gases Emissions and other basic steps, Combining the above basic steps turnning into the ammonia synthesis reaction and recycling process , in which ammonia synthesis section is the central part of a synthetic ammonia process.The task of curriculum design is the ammonia synthesis section of an annual three hundred thousand tons synthetic ammonia plant . The composition of fresh feed gas is: H2(74.5%),N2(24%),CH4(1.2%),Ar(0.3%), the inlet gas composition of the Reactor is : NH3(2.5%),CH4+Ar(17%),it Requires the mole fraction of ammonia reacheds to 13.2% of outlet gas of synthesis reactor. By consulting the relevant literature and information,we designed the ammonia synthesis section of an annual three hundred thousand tons synthetic ammonia plant, and we did the material balance accounting , energy balance accounting and the equipment selection and calculation. Finally, with the help of CAD technology,we draw the process flow diagram and the heat exchanger equipment diagram. Keywords: ammonia synthesis section material balance accounting energ