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槟榔炒制“火候”量化及其规律分析-quantification and analysis of
3.2.4 专属性考察...................................................................................................613.2.5 色谱条件的选择...........................................................................................6 流动相的选择....................................................................................6 色谱柱的选择....................................................................................623.2.6 标准曲线的制备及最低检出限...................................................................633.2.6 精密度试验...................................................................................................643.2.7 样品稳定性试验...........................................................................................643.2.8 重复性试验...................................................................................................653.2.9 加样回收试验...............................................................................................663.3 动力学研究样品制备方法学考察..........................................................................673.3.1 样品炒制方法的考察...................................................................................673.3.2 不同时间点样品制备方法考察...................................................................673.4 槟榔炒制样品制备及取样设计..............................................................................683.4.1 收得率测定设计...........................................................................................683.4.2 动力学研究样品制备设计...........................................................................683.5 样品含量测定结果及数据处理..............................................................................693.5.1 槟榔生品含量测定结果...............................................................................693.5.2 炒制过程相关参数测定结果及数据处理...................................................693.5.3 数据分析及建立动力学数学模型...............................................................733.6 结论..........................................................................................................................793.6.1 在
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