固态高聚物动静态黏弹性的实验分析-experimental analysis of dynamic and static viscoelasticity of solid polymer.docxVIP

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固态高聚物动静态黏弹性的实验分析-experimental analysis of dynamic and static viscoelasticity of solid polymer.docx

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固态高聚物动静态黏弹性的实验分析-experimental analysis of dynamic and static viscoelasticity of solid polymer

湘潭大湘潭大学硕士学位论文ABSTRACTPolymers are typically viscoelastic in nature, their viscoelastic properties are essential in investigating their mechanical performances. Viscoelasticity is normally classified into two types, static viscoelasticity and dynamic viscoelasticity. The main influence factors of static and dynamic viscoelastic properties of the polymers include temperature, stress, load frequency, strain and physical aging, etc.. In this thesis, the general viscoelasticity of polymer solids and the time-temperature superposition are introduced in the first part, the effects of temperature, stress, physical aging on the static viscoelastic properties of PMMA are discussed in the second chapter, and the influences of temp erature, strain frequency, strain amplitude and physical aging on the dynamic viscoelastic properties of rubber and PC are investigated in detail in the final chapter. Several conclusions can be drawn as follows:The short-term creep tests of PMMA are conducted under different temperatures and stresses. The isochronous creep rate of the material is found to increase with temperature. It is shown that based on the time-temperature superposition, the 4000 s’creep data gotten at 26MPa and 26℃ can be used to predict the creep property up to46 days, which is much longer than the test duration, at 14℃ and the same stress. This indicates the time-temperature superposition provides a way of accelerated characterization of long-term creep behavior. The tests also show that there exists a critical stress at which nonlinear viscoelasticity occurs, and moreover this critical stress decreases with temperature.The constant strain rate tensile tests are performed on PMMA specimens aged to different periods of time. It is shown that both the initial instantaneous elastic modulus and the fracture stress of the material increase with aging time and approach to their asymptotic values, which satisfy the Kohlrausch-Williams-Watts(KWW) rule. Meanwhile, the creep tests