铝二次电池离子液体电解液及介孔炭硫正极材料的分析-analysis of ionic liquid electrolyte and mesoporous carbon-sulfur cathode materials for aluminum secondary batteries.docxVIP

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铝二次电池离子液体电解液及介孔炭硫正极材料的分析-analysis of ionic liquid electrolyte and mesoporous carbon-sulfur cathode materials for aluminum secondary batteries.docx

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铝二次电池离子液体电解液及介孔炭硫正极材料的分析-analysis of ionic liquid electrolyte and mesoporous carbon-sulfur cathode materials for aluminum secondary batteries

原理工大学硕士研究生学位论文原理工大学硕士研究生学位论文 THE STUDY ON IONIC LIQUID ELECTROLYTE AND ORDERED MESOPOROUS CARBONS / SULFUR CATHODE MATERIAL 卧J SECONDARY ALlTh哑NU孔，f BATIERY ABSTRACT Aluminum secondary battery is a new generation of chemica l power suppl弘 after the second lead-acid batteries，nickel cadmium batteries，nickel metal hydride batteries and lithium secondary battery. Compared with other secondary battery systems，aluminum secondary battery have characteristics of higher energy，lower cost，lighter weight，smaller，more environmentally friendly，safe and stable，cost-effective and so on. Based on the theoretica l system of aluminum secondary battery，ionic liquids electrolytes are studyed. One-step preparation with AICI ytrielhylam ine hydrochloride liquid ，and the cyclic voltammetry and conductivity tests，to study the eleclrochem ical stability window，the conductivity curve with temperature ， thermal stability and the mecbanism of deposition and dissolution of aluminum 缸e studyed. On this basis，various organic solvents on the improvement of the electrolyte are studied. In the PC，THF，DCE，EC，DCE and EC are optimized. Tben by adding 8% DCE +2% EC，7% DCE + 3% EC，6% DCE +4% EC，5% lIIDCE +5% EC，different organic solvents on the improvement of the electrolyte l I I 太原理工大学硕士研究生学位论文 are studyed. The mesoporous carbon/sulfur cornposite as cathode materials for secondary aluminum battery is studyed. Soft t， nplate synthesis of mesoporous carbon materials，the XRD spectra，SEM of sulfur compound before and after， BET changes in different proportion s are study创. Mesoporous carbon of the sulfur composite cathode materials，to 7% DCE +3% EC diluted AJCh/triethylamin e hydrochloride ionic liquid as electrolyte， composed of high purity aluminum for the aluminum anode secondary batteries， do Charge-discharge tests and by comparing the different mesoporous carbon and sulfur in the compound ratio of the impact of battery capacity，then of different binders on 出e impac