难钝化不锈钢钝化技术分析-analysis of passivation technology for stainless steel that is difficult to passivate.docxVIP

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难钝化不锈钢钝化技术分析-analysis of passivation technology for stainless steel that is difficult to passivate.docx

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难钝化不锈钢钝化技术分析-analysis of passivation technology for stainless steel that is difficult to passivate

AbstractFreecuttingstainlesssteelhasbeenwidelyusedindecorationindustriesforitsexcellentmechanicalandmachiningproperties.Topreventcorrosionofthestainlesssteelornaments,passivationisagoodway,usuallynitricacidandchromatecanbeemployed.However,passivitybychromateisharmfultotheenvironmentandhasbeenrestricted;nitricacidmethodisdifficulttoobtainpassivefilmwithgoodperformancebytheactiveinclusionswhichcomefromtheintroductionofcuttingelements.Soakindofefficientandenvironmentfriendlypassivationsolutionisquitenecessary.Citricacidpassivation,withappropriatepre-treatmentandpost-processing,iseffectiveandverypromisingforenvironmentalprotection.Inthispaper,weuseddifferentpassiveformulasforrapidscreeningbytheimprovedbluedotmethodandthenwehavefoundthatthepassivationbycitricacidsolutionasthemostsuccessful.Withorthogonaltestforcitricacidpassivationprocessforfurtheroptimization,measurementandanalysisoftheTafelcurveofthepassivationtreatmentbythepolarizationresistanceRpvalue,aprocessofcitricacidpassivationisdeveloped.Inordertoenhancetheeffectoffreecuttingsteelpassivation,avarietyofpre-treatmentwayshasbeentested.Bymeansofthebluedotmethod,Tafelcurveanddynamicpotentialscanning,tohavedeterminedtheHF+H2SO4+FA,HF+H2SO4+CA,FKpre-treatmentwayswithaverygoodpassivationeffect.Lastexaminethepost-processingpassivationeffectofHNO3underdifferenttimes,theresultsshowthattheeffectofnitricacidpassivationtreatmentisfirsttoincreasethendecrease,thebestpost-processingtimefornitricacidis5min.Alsotesttheeffectofsilicatesealingtreatment,findthattodrysilicatefilmsat200℃getmuchbetteranticorrosioneffect,butnotconducivetotheactualoperationandcostcontrol.JointpassivationeffectshowsthatthejointapproachFKpassivationbeentestedinferricchloridesolution,theneutralsaltspraytest,Tafelcurveshowagoodresistancetocorrosionandpitting.Theneutralsaltspraytestshowsmuchbettereffectthanhighsulfur-type-specificchromateformulaforfreecuttingstainlesssteelpassivation.Itisakindofnewmoreenvironmentallyfriendly,efficientandeffectivefreecuttingst