模拟csp工艺制备hi-b钢初次及二次再结晶研究-study on primary and secondary recrystallization of hi - b steel prepared by simulated csp process.docxVIP

II II Abstract The research of Hi-B steel produced by CSP technology has attracted great attention, because of the problems of traditional process such as the high cost and high energy consumption. CSP technology was simulated to product Hi-B steel in laboratory, and a range of experiments from steelmaking to secondary recrystallization annealing were designed. Evolution of microstructure and texture in the primary and secondary recrystallization annealing process of Hi-B steel were studied by EBSD and XRD technique, also effects of different process on secondary recrystallization were discussed. The main results are as follows: The primary recrystallization of Hi-B steel finished in 15s at 830℃. With the increasing of annealing time, the grain size gradually grew up, the proportion of Σ1 interface decreased, but the proportion of Σ3~Σ9 interface proportion did not change much, while misorientation distributions changed into a majority of high angle grain boundaries. Abnormal growth of goss grains occurred in 1100℃ with the heating rate of 20℃/h during the process of high-temperature annealing, the behavior of its growth was different from normal grain growth. After abnormal growth, goss grains had size advantage, goss texture dominated the texture component gradually. Secongdary recrystallization of Hi-B steel was divided into three stages, namely early stage of slowing growth, intermediate stage of preferred growth and the final stage of swallowing island grains. At different stage, the mechanism of growth of goss grains was different. Cold rolling reduction, normalizing and heating rate affect the evolution of goss texture. The reduction, either too large or too small, was not conducive to the abnormal growth of goss grains. A lot of AlN particles, which almost didn’t precipitate during hot rolling, precipitated during normalizing. This change had no obvious effect on microstucture and texture of primary recrystallization, however, it greatly improved the III