锑酸银和铌酸银及其复合体系的表面光电和光催化性能分析-analysis of surface photoelectric and photocatalytic properties of silver antimonate, silver niobate and their composite systems.docxVIP

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锑酸银和铌酸银及其复合体系的表面光电和光催化性能分析-analysis of surface photoelectric and photocatalytic properties of silver antimonate, silver niobate and their composite systems.docx

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锑酸银和铌酸银及其复合体系的表面光电和光催化性能分析-analysis of surface photoelectric and photocatalytic properties of silver antimonate, silver niobate and their composite systems

samples of AN170, AN180, AN190, AN200 and AN240 are obtained. Their phases, surface morphology and surface photovoltaic property were characterized by X-ray diffraction, UV-visible spectrophotometer, Raman scattering, scanning electron microscopy and surface photovoltage spectroscopy. The photocatalytic property was estimated by degradation of Rhodamine B. The results show that different morphologies may be due to different morphologies of Ag particles and that AN190 with the weakest photovoltage and the highest photocatalytic activity may be due to synergetic effect between silver niobate and Nb2O5. Both the temperature and the amount of Nb2O5 are crucial for the morphologies, the photoelectric and photocatalytic properties of the samples. 3) The compound with different molar ratio of silver niobium and sodium antimony were prepared by solid state reaction method. Firstly, appropriate amount Ag2O，Sb2O3, Na2CO3 and Nb2O5 were well mixed respectively, then are calcained at 750 oC for 4 hours and 900 oC for 8 hours in turn. The samples of xAgSbO3/NaNO3 （x=0.5, 1.0, 2.0, 4.0, 6.0）are obtained. Their phases, surface morphology and surface photovoltaic property were characterized by X-ray diffraction, UV-visible spectrophotometer, Raman scattering, scanning electron microscopy and surface photovoltage spectroscopy. The photocatalytic property is estimated by degradation of Rhodamine B. The results show that the surface photovoltage and photocatalytic activities were sensitive to the molar percentage of sodium antimony in the samples; the highest photocatalytic activity was observed on the composite of silver niobium and sodium antimony due to the better dispersiveness, electron transfer and surface photoelectric properties, these results indicate that making the composite is an effective method to modify the photophysical and photochemical properties of photocatalyst. KEY WORDS: Silver antimony, Silver niobate, Composite, Surface photovoltage, Photocatalytic ac