不同热处理对牙科铸造银钯合金腐蚀行为影响.docVIP

不同热处理对牙科铸造银钯合金腐蚀行为的影响 　　[文章编号] 1000-1182(2014)03-0238-04 　　[摘要] 目的 研究不同处理对牙科用银钯铸造合金腐蚀行为的影响。方法 熔炼银钯铸造合金，参照ISO 10271:2001牙科金属材料抗腐蚀实验标准，按照标准牙科失蜡法铸造程序制作测试样本，经固溶软化处理后，分别进行相应的热处理、深冷处理、热处理并深冷处理，以固溶软化处理组作为对照组。采用金相显微镜观察分析，并行电化学实验、静态浸泡实验测试合金的电化学参数及非贵金属离子析出值。结果 各实验组的金相结构发生了变化，电化学参数的开路电位Eocp、腐蚀电位Ecorr及腐蚀电流密度Icorr与对照组的差异有统计学意义（P0.05）。结论 各组的抗腐蚀性能指标均能满足ISO标准的要求，适当的热处理、深冷处理、热处理并深冷处理能改善实验合金的抗腐蚀性能。 　　[关键词] 牙科银钯铸造合金；热处理；深冷处理；金相结构；腐蚀行为 　　[中图分类号]R 783.1 [文献标志码] A [doi] 10.7518/hxkq.2014.03.007 　　 　　Influence of cryogenic treatment and age-hardening heat treatment on the corrosion behavior of a dental casting Ag-Pd alloy Zhao Yao1,2, Wu Bin3, Meng Yukun1. (1. State Key Laboratory of Oral Diseases, Dept. of Prosthodontics, West China Hospital of Stomatology, Sichuan University, Chengdu 610041, China; 2. Chongqing Key Laboratory for Oral Diseases and Biomedical Sciences, Dept. of Prosthodontics, The Affiliated Hospital of Stomatology, Chongqing Medical University, Chong-qing 401147, China; 3. Dept. of Stomatology, Longhua People’s Hospital in Baoan District, Shenzhen 518109, China) 　　[Abstract] Objective The purpose of this study is to investigate the influence of cryogenic treatment and age-hardening heat treatment on the corrosion behavior of a dental casting Ag-Pd alloy. Methods A low gold content dental casting alloy composed of Ag-Pd-Cu-Au was prepared for this study. Corrosion test was performed according to ISO 10271:2001 dental metallie-corrosion test methods. Experimental specimens were casted according to a standard dental lost-wax casting procedure, treated with solution by heating the specimens to 900 ℃, and immediately quenched in ice water. The specimens were then divided into four groups and subjected to heat treatment, cryogenic treatment, and heat treatment combined with cryogenic treatment. The specimens after the solution treatment were taken as control. The metallographic structures of the specimens were ob-served. The electrochemical parameters and the quantity