薄荷油微胶囊的制备及其应用-材料工程专业论文.docxVIP

东华大学硕士学位论文摘要 东华大学硕士学位论文 摘要 ii ii 控剂用量为 5wt％，螺杆、组件、喷丝板温度分别为 250℃、265℃、 238℃。实验结果表明，尼龙 6 的可纺性与微胶囊含量有关系，随着 微胶囊含量的增加，可纺性降低，由于微胶囊的加入，尼龙 6 纤维的 物理机械性能有所下降，纤维含油率虽然不高，但是有明显的芳香效 果，且薄荷油释放速率缓慢，有留香效果。 将微胶囊化的薄荷油通过浸轧方式整理棉织物，通过对棉织物含 油率，力学性能，硬挺性，折皱回复角，白度，表面形貌的研究，微 胶囊浸轧整理棉织物的最佳工艺条件为：预烘温度为 70℃，预烘时 间为 3min，焙烘温度为 120℃，焙烘时间为 2min。通过扫描电镜（SEM） 分析，经整理的棉织物表面和纤维空隙中均能观察到微胶囊的存在， 并且大部分的微胶囊形态完整，没有破壁现象。通过含油率的分析， 存在于棉织物中的微胶囊释放薄荷油速率缓慢，有一定的缓释作用。 关键词：薄荷油；微胶囊；制备；熔融纺丝；浸轧整理 东华大学硕士学位论文Ab 东华大学硕士学位论文 Abstract PAGE PAGE iii PREPARATION AND APPLICATION OF THE PEPPERMINT OIL MICROCAPSULES ABSTRACT Most of the essential oils such as peppermint oil are easy to volatilize because of their low boiling points, as a resutl the essential oils can hardly bear the processing temperature when incorporating them into fibers to manfacture fragrant fabric. Moreover, the fragrant duration will be short because of the quick evaporation of essential oil. As a matter of fact, this problem could be overcome partly by using the technique of microcapsulation. Enwrapping essential oil with suitable wall materials can not only protect it from the relatively high processing temperature, but also restrict its evaporation to achieve the slow-release effect. In this paper, the peppermint oil microcapsules with slow-release effect were prepared by complex coacervation method, using gelatin and arabic gum as the wall materials and pepepermint oil as the core material. And then the obtained peppermint oil microcapsules were incorporated into nylon6 fiber and cotton fabric respebtively by means of blend melt spinning and padding finish. The properties of fibers and cotton fabric were studied. The main content of this paper is as follow： The peppermint oil microcapsules were prepared using complex coacervation method. The process parameters, such as the concentration of emulsifier, the dosage of cross linker, the stirring speed, the concentration of wall materials, the ratio between core and wall materials and the pH value of coacervatio