基于挥发性特征组分的卷烟烟丝质量趋势分析..docVIP

基于挥发性特征组分的卷烟烟丝质量趋 势分析 李超刘秀明秦云华王家俊张承明李娥贤许永 云南中烟工业有限责任公司技术中心卷烟产品质量 检测中心云南省农业科学研究院生物技术与种质资 源研宄所 为考察卷烟烟丝的质量变化趋势，采用顶空气相色谱质谱联用法（HS-GC/MS） 检测不同品牌、不同批次卷烟烟丝中50种挥发性特征组分含量（质量分数），结 合主成分分析-马氐距离（PCA-MD）统计方法对检测数据进行处理并进行质量趋 势分析。结果表明：（1） C品牌5个批次卷烟烟丝样品可分成5类，K2015与 2016年烟丝特征组分含量波动较大;2016年7—10月份的烟丝屮50种挥发性特 征组分含量基本一致，仅8月份出现细微波动。该变化趋势与烟丝配方调整的情 况一致。（2） 2015年C、D品牌烟丝样品中特征组分含量的差异较大，表明可 以用PCA对不同品牌质量特征进行定性描述。（3） C、D品牌烟丝样品间的马氏 距离较大，D品牌的马氏距离是C品牌的510倍，表明可以用马氏距离对卷烟烟 丝质量波动状况进行定量表征。该研宂结果可用于卷烟产品的均质化评价。 关键词： 卷烟烟丝;挥发性特征组分;主成分分析-马氏距离;质量趋势分析;均质化评 李超（1985—），硕士，工程师，主要从事烟草化学、应用统计学研 光。 : supcr88man66@126. com; 蒋次清， : jiangcq@ynzy_tobacco. com 2017-02-13 基金：云南中烟工业有限责任公司2015年重点项目“适用于卷烟产品质量管控 的分析检测平台搭建及应用” （2015JC07） Quality trend analysis on cigarette cut filler based on characteristic volatile components in cut filler LI Chao LIU Xiuming QIN Yunhua WANG Jiajun ZHANG Chengming LI Exian XU Yong WU Yiqin JIANG Ciqing Cigarette Product Quality Test Center， Technology Center of China Tobacco Yunnan Industrial Co.，Ltd, ; Institute of Biotechnology and Genetic Resources， Yunnan Academy of Agricultural Sciences; Abstract： To investigate the variations in quality trend of cigarette cut fillers, HS-GC/MS was used to determine the contents of 50 volatile characteristic components in cut fillers of cigarettes of different batches and brands. By combining PCA-MD (Principal component analysis-Mahalanobis distance) statistical methods, the determined data were processed to analyze the variation trend of quality of cut filler. The results showed that: 1) The cut fillers of cigarettes of five batches of brand C could be classified into five groups, the contents of characteristic components differed greatly between the samples produced in 2015 and 2016. From July to October in 2016，the contents of 50 volatile characteristic components in the cut fillers were basically consistent except that there was slight fluctuation in August, which could be attributed to the tobacco blend adjustment. 2) For the samples produced in 201