《原子吸收法测定矿石中铜的测量不确定度评定》-毕业论文.docVIP

精品 毕 业 设 计 （论文） 原子吸收法测定矿石中铜的测量不确定度评定 英文题目: Evaluation of the Uncertainty in the Determination of Copper in Ore by AAS 姓 名: 学 号: 指导教师: 教授 专 业: 应用化学 二零一二年六月 精品 东华理工大学毕业设计（论文） 绪论 PAGE 1 22 摘 要 　　本文研究分析了原子吸收分光光度法测定矿石中铜的过程，并建立了其检测方法相应测量不确定度评定的数学模型。在所建立的模型中对各个参数进行分析结果测量不确定度的误差来源分析，对于A类不确定度(即由测量的结果统计分布计算引入的测量不确定度)与B类不确定度(即基于经验或其他信息的概率分布估计引入的测量不确定度)进行评定，然后参照标准对各个测量不确定度分量合成和扩展，最终进行该方法的测量不确定度评定。本研究结果表明：AAS法测定矿石中铜的检测方法，其测量不确定度的误差主要来源为：标准曲线拟合线性方程、标准溶液的配制及样品溶液的定容。 关键词：原子吸收光谱法； 不确定度； 铜含量 ABSTRACT 　In this paper, the Atomic Absorption Spectrometry determination of copper in the ore, and the establishment of the detection method is the appropriate mathematical model of Measurement Uncertainty in Sources of error of measurement uncertainty analysis of the various parameters in the model analysis, for the Class A uncertainty ( by measuring the results of the statistical distribution of the calculation of measurement uncertainty) and the introduction of Class B uncertainty (the distribution of the measurement uncertainty is estimated that the introduction of probability based on experience or other information) to be assessed, and then refer to the standard component synthesis and extension of each measurement uncertainty, and ultimately the methods of measurement uncertainty Evaluation. The results of this study show that: AAS detection method for determination of copper in the ore, the main error sources of measurement uncertainty: standard curve fitting a linear equation, the standard solution and sample solution constant volume. Keywords：Atomic Absorption Spectrometry (AAS); Uncertainty; Copper 精品 目 录 TOC \o 1-3 \h \u HYPERLINK \l _Toc10000 1 绪论 PAGEREF _Toc10000 1 HYPERLINK \l _Toc30932 1.1 测量不确定度的历史、现状及重要意义 PAGEREF _Toc30932 2 HYPERLINK \l _Toc2512 1.2 评定不确定度测量的两种方法 PAGEREF _Toc2512 4 HYPERLINK \l _Toc28920 1.