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- 2018-11-20 发布于广西
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摘 要
葡萄皮渣中含多种有益物质,如原花青素、白芦醇、葡萄籽油等,这些物质具有较好的医疗保健作用。从中提取果胶、酒石酸、芳香物质、膳食等,可应用于食品工业[1]。本文针对于葡萄皮渣中提取d-酒石酸的工艺条件的研究。首先由静态吸附动力学曲线对D301R、D201、D296、201×7四种离子交换树脂进行筛选,得出最佳离子交换树脂为D301R。用D301R树脂进行静态吸附,研究其静态吸附的温度、pH、最佳吸附时间。同时研究其动态解吸的解吸液的体积、浓度、流速对解吸率的影响。得出其最佳工艺条件,静态吸附的最佳工艺条件:吸附时间为7小时,温度为35℃,pH为3.00;动态解吸的最佳工艺条件解吸液体积为4BV,解吸液流速为3BV/h,解吸液浓度为15%NaCl。本实验采用偏钒酸钠比色法对酒石酸含量进行测定,测得其标准曲线回归方程为Y=3.2676x-0.0139,R2=0.9976。
关键词:葡萄皮渣,酒石酸,提取,工艺条件的研究
ABSTRACT
Grape skins slag containing many beneficial substances, such as procyanidins, white reed alcohol, grape seed oil etc., these material has good health care function. Extract pectin, tartaric acid, aromatic substances, dietary etc, can be applied to the food industry . This paper extracted from grape skins - tartaric acid slag technological conditions of the d. By static adsorption kinetic curve first D301R, D201 to D296, 201 x 7, four kinds of ion exchange resin, obtains the best screening for D301R ion exchange resin. Static adsorption resin with D301R, studies its static adsorption temperature, pH, best adsorption time. Meanwhile research on its dynamic desorption the volume of the desorption liquid, the concentration, the influence of flow rate of desorption. Draw the optimum technological conditions for static adsorption the optimum technological conditions: for seven hours, adsorption time for 35 ℃ temperature, pH value for 3.00; The optimum process conditions of dynamic desorption product, 4BV desorption liquid 3BV/desorption fluid velocity h, desorption liquid concentration of 15% NaCl. This experiment used slant vanadium acid sodium colorimetric determination of tartaric acid content, the measurement standard curve regression equation is Y = 3.2676 x - 0.0139 R2 = 0.9976
Key words: grape skins slag, tartaric acid, extraction, the research process conditions
目 录
TOC \o 1-3 \h \u HYPERLINK \l _Toc3705 前 言 PAGEREF _Toc3705 5
HYPERLINK \l _Toc31809 第一章 文章综述 PAGEREF _Toc31809 6
HYPERLINK \l _Toc9277 1.1葡萄及葡萄皮渣简介 P
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