土壤样品前处理——微波消解研究探究.pdfVIP

Advances in Environmental Protection 环境保护前沿, 2017, 7(2), 170-179 Published Online April 2017 in Hans. /journal/aep /10.12677/aep.2017.72025 Pretreatment of Soil Sample—Microwave Digestion 1,2 1 2* Ting Gao , Xuanping Yang , Wenxiang Hu 1 Beijing Xianghu Science and Technology Development Co., LTD, Beijing 2 Jingdong Xianghu Laboratory of Beijing Excalibur Space Military Academy of Medical Sciences, Beijing t h th th Received: Apr. 12 , 2017; accepted: Apr. 27 , 2017; published: Apr. 30 , 2017 Abstract The soil samples were digested by one-time microwave digestion method, and the better digestion condition was found. The results showed that the digestion effect of nitric acid - hydrochloric acid - hydrofluoric acid system and nitric acid - hydrogen peroxide - hydrofluoric acid system were the same when the soil sample was 0.1000 g. The former method was better than the latter one when the soil sample was 0.1500 g. Therefore, it was recommended to choose the nitric acid - hydroch- loric acid - hydrofluoric acid system in soil microwave digestion. The higher the purity of the acid, the better the accuracy of the test. Keywords Microwave Digestion, Soil, Sample Pretreatment, Xianghu Microwave Digestion Instrument 土壤样品前处理——微波消解研究 1,2 1 2* 高 婷 ，杨萱平 ，胡文祥 1北京祥鹄科技发展有限公司，北京 2北京神剑天军医学科学院京东祥鹄实验室，北京 收稿日期：2017年4月12 日；录用日期：2017年4月27 日；发布日期：2017年4月30 日 摘 要 采用微波消解的办法，对土壤样品进行一次性消解处理，以期找到较优消解条件，将土壤消解完全。结 果发现土壤称样量0.1000 g时，用硝酸–盐酸–氢氟酸体系和硝酸–过氧化氢–氢氟酸体系消解效果相 *通讯作者。 文章引用: 高婷, 杨萱平, 胡文祥. 土壤样品前处理——微波消解研究[J]. 环境保护前沿, 2017, 7(2): 170-179. /10.12677/aep.2017.72025