地龙β-环糊精包合除味工艺研究.PDFVIP

网络出版时间：2012-11-26 18:01 网络出版地址：/kcms/detail/12.1108.R1801.009.html 地龙 β-环糊精包合除味工艺研究 王 昶，魏文峰，张树明，王伟明* 黑龙江省中医研究院，黑龙江 哈尔滨 150036 摘 要：目的 制备地龙 β-环糊精包合物，改善其溶解性及去除不良气味。方法 以次黄嘌呤为指标，考察 β-环糊精加入 比例、温度及时间对包合工艺的影响，并进行包合物口感满意度及溶解性检测。结果 在地龙（生药）-β-环糊精的比例为 15 ∶1，70 ℃下超声处理 60 min，次黄嘌呤平均包合率为 80.31%，口感满意率为 90% 以上，溶解度有较大改善。结论 地 龙 β-环糊精包合工艺可行，并可有效解决地龙不良气味问题。 关键词：地龙；β-环糊精；次黄嘌呤；口感满意度；不良气味 中图分类号：R283.6 文献标志码：A 文章编号：0253 - 2670(2013)03 - 0000 - 00 Study on arthworm and β-cyclodextrin inclusion for odor removal WANG Chang, WEI Wen-feng, ZHANG Shu-ming, WANG Wei-ming Heilongjiang academy of TCM, Heilongjiang 150036 Abstract: Objective To prepare the inclusion compound of earthworm/β-cyclodextrin with improved solubility and removed bad smell. Methods The effects of the proportion between arthworm and β-cyeiodextrin, inclusion temperature and time were considered as influenting factors and with the hypoxanthine as indicator. And the satisfaction and solubility of inculsion were tested. Results The optimal process was as follows: the earthworm (pharmacognosy)-β-cyclodextrin is 15:1, ultrasonic treatment is 60 minutes under 70 ℃, the inclusion rate of hypoxanthine is 80.31% from the above method, the taste satisfaction rate is 90%, the solubility is greatly improved. Conclusion The inclusion process is feasible and the earthworm bad odor problem were solved effectively. Key words: earthworm; β-cyclodextrin; hypoxanthine; satisfaction; earthworm bad odor 地龙为环节动物门钜蚓科动物参环毛蚓 化仪器厂），UV—160 紫外分光光度计（日本岛津 Pheretimaas pergilum (E Perrier) 、通俗环毛蚓 P. 公司）。广地龙Pheretimaas pergilum (E Perrier) （广 vulgaris Chen 、威廉环毛蚓P. guillelmi (Michaelsen) 东，采集时间 2007.08 ），经黑龙江省中