ALN-SiC复合陶赞瓷的衰减性能.docVIP

AlN-SiC复合陶瓷的微波衰减性能的研究 张玉利1）， 贾成厂1）*， 高鹏1） (1）北京科技大学材料科学与工程学院，北京，100083) 摘要：以氮化铝，纳米碳化硅为原料，无烧结助剂， 1600℃,，30MPa下，保温5min，放电等离子体烧结（SPS），制备了AlN-SiC复合陶瓷。分别利用扫描电镜，能谱分析仪，XRD，安捷伦4284ALRC阻抗分析仪等对其致密度，显微结构，表面成分，生成的主要物相，介电损耗和介电性能进行分析。分析结果表明:，AlN-SiC复合陶瓷的致密度在93%以上，物相主要有作为原料的AlN和β-SiC，以及烧结之后生成的2H-SiC和Fe5Si3，随着SiC含量的增加，材料的介电损耗，介电常数相应增加，SiC含量在30%-40%wt之间，1MHz以下的损耗角正切tanδ≥0.3。为此表明纳米SiC具有较强的吸波性能。相同含量的碳化硅，材料的介电常数和介电损耗随着频率的增加而降低，。XRD结果分析可知，除原料AlN和β-SiC以外，有部分2H-SiC和Fe5Si3生成，烧结之后的AlN-SiC复合陶瓷的致密度在93%以上。 关键词：氮化铝，纳米碳化硅，SPS，介电损耗 Study on Performance of AlN-SiC Composite Ceramics with Attenuation Characteristics请对英文摘要做相应的修改。 请对英文摘要做相应的修改。 ZHANG Yuli1）， JIA Chengchang1）*，GAO Peng1） (College of Materials Science and Engineering , Beijing University of Science and Technology, Beijing, 100083) Abstract：AlN-SiC composites with AlN and nanoβ-SiC as raw materials were prepared by SPS at the temperature of 1600, 30MPa uniaxial pressure and soaking time for 5min without any sintering additives in a vacuum atmosphere. The microstructure, the produced phases，dielectric constant and loss tangent of the ceramics were characterized by scanning electron microscopy，XRD, and Agilent4284A LCR automatic tester respectively. The results show the loss tangent and dielectric constant are increased by the SiC content increasing. The loss tangent is more than 0.3 with the SiC content ranging from 30-40wt%. It’s indicated that nanometer SiC has strong absorbing property. We also know that the dielectric constant and dielectric loss are deduced by the frequency increasing with the same content of silicon carbide. In addition to AlN and beta SiC, 2H-SiC and Fe5Si3 are generated with the aid of the XRD analysis. The relative densities of sintered ceramics are in excess of 93%. Key words: aluminum nitride; nano HYPERLINK app:ds:siliconsilicon HYPERLINK app:ds:carbidecarbide; SPS；dielectric loss 基金项目：中俄国际合作项目，功率微波电真空器件用高热导陶瓷材料，2010DFR50360 通讯通信作者：贾成厂，教授，博士生导师，主要从事复合材料，粉末冶金的研究 E-mail：jcc@ustb.edu.cn 引言 吸波材料广泛应用于军事领域，主要用作大功