液相色谱-串联质谱法测定蜂蜜中8种大环内酯类药物残留的不确定度.PDF

8 5 Vol. 8 No. 5 2017 5 Journal of Food Safety and Quality May. , 2017 -8 1, 2 1 2 1 2 2* 申雪丽 , 陈 瑞 , 周靓静 , 莫卫民 , 钱鸣蓉 , 吴俐勤 (1. , 310014; 2. , 310021) 摘 要: 目的 -(liquid chromatography-tandem mass spectrometry, LC-MS/MS) 8 方法 JJF1059.1-2012 , LC-MS/MS , , , 结果 k=2 , : (9.02±0.81)(9.26±0.63)(9.79±0.68)(9.47±0.59) (9.75±0.82)(9.16±0.70)(9.59±0.60)(9.84±0.68) µg/kg结论 ; , , 关键词: ; ; -; Uncertainty evaluation for determination of 8 kinds of macrolide residues in honey by liquid chromatography-tandem mass spectrometry 1, 2 1, 2 2 1 2 2* SHEN Xue-Li , CHEN Rui , ZHOU Liang-Jing , MO Wei-Min , QIAN Ming-Rong , WU Li-Qin (1. College of Chemical Engineering, Zhejiang University of Technology, Hangzhou 310014, China; 2. Institute of Quality and Standard on Agricultural Products, Zhejiang Academy of Agricultural Sciences , Hangzhou 310021, China) ABSTRACT: Objective To evaluate the measurement uncertainty for determination of macrolide residues in honey by liquid chromatography-tandem mass spectrometry (LC-MS/MS). Methods According to JJF